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6-甲氧基喹啉

产品名称 6-甲氧基喹啉

CAS号5263-87-6

分子式C10H9NO

分子量159.18

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  • Mass

    MS-NW-7299          
    6-methoxyquinoline
    C10H9NO             (Mass of molecular ion:    159)
    

       Source Temperature: 200 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          38.0       1.7
          39.0       3.7
          50.0       2.6
          51.0       3.0
          52.0       1.5
          61.0       1.1
          62.0       4.0
          63.0       9.0
          64.0       2.3
          65.0       1.2
          74.0       2.4
          75.0       3.2
          76.0       1.7
          77.0       2.2
          79.5       2.1
          87.0       1.2
          88.0       2.7
          89.0      17.1
          90.0       3.4
         101.0       2.8
         102.0       3.4
         103.0       1.1
         114.0       1.0
         115.0       1.9
         116.0      66.9
         117.0       6.6
         128.0       4.3
         129.0      14.3
         130.0       5.1
         144.0      11.4
         145.0       1.5
         158.0       1.2
         159.0     100.0
         160.0      11.8
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C10 H9 N O 0.05 ml : 0.5 ml CDCl3
    6-methoxyquinoline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.731 B 7.98 C 7.95 D 7.33 E 7.28 F 6.982 G 3.864

         Hz     ppm     Int.
    

        784.94   8.765     82
        783.31   8.747     88
        780.69   8.717     89
        779.06   8.699     89
        720.56   8.046     96
        717.94   8.017     62
        716.44   8.000     60
        716.06   7.996     60
        711.38   7.944    141
        709.88   7.927     89
        708.06   7.906     78
        662.94   7.403     93
        660.13   7.371    108
        657.19   7.338    109
        653.69   7.299     99
        652.94   7.291    113
        650.94   7.269    101
        648.88   7.246     81
        644.56   7.197     71
        626.44   6.995    137
        623.75   6.965    119
        344.50   3.847   1000
    

in CDCl3



liquid film