6-甲氧基喹啉

产品名称 6-甲氧基喹啉

CAS号5263-87-6

分子式C10H9NO

分子量159.18

¹³CNMR

Mass

MS-NW-7299          
6-methoxyquinoline
C10H9NO             (Mass of molecular ion:    159)

   Source Temperature: 200 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      38.0       1.7
      39.0       3.7
      50.0       2.6
      51.0       3.0
      52.0       1.5
      61.0       1.1
      62.0       4.0
      63.0       9.0
      64.0       2.3
      65.0       1.2
      74.0       2.4
      75.0       3.2
      76.0       1.7
      77.0       2.2
      79.5       2.1
      87.0       1.2
      88.0       2.7
      89.0      17.1
      90.0       3.4
     101.0       2.8
     102.0       3.4
     103.0       1.1
     114.0       1.0
     115.0       1.9
     116.0      66.9
     117.0       6.6
     128.0       4.3
     129.0      14.3
     130.0       5.1
     144.0      11.4
     145.0       1.5
     158.0       1.2
     159.0     100.0
     160.0      11.8

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₉ N O	0.05 ml : 0.5 ml CDCl₃
6-methoxyquinoline

    Assign.     Shift(ppm)

      A             8.731
      B             7.98
      C             7.95
      D             7.33
      E             7.28
      F             6.982
      G             3.864

     Hz     ppm     Int.

    784.94   8.765     82
    783.31   8.747     88
    780.69   8.717     89
    779.06   8.699     89
    720.56   8.046     96
    717.94   8.017     62
    716.44   8.000     60
    716.06   7.996     60
    711.38   7.944    141
    709.88   7.927     89
    708.06   7.906     78
    662.94   7.403     93
    660.13   7.371    108
    657.19   7.338    109
    653.69   7.299     99
    652.94   7.291    113
    650.94   7.269    101
    648.88   7.246     81
    644.56   7.197     71
    626.44   6.995    137
    623.75   6.965    119
    344.50   3.847   1000

in CDCl3

liquid film

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