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MassMS-IW-1768 2-chloro-5-(trifluoromethyl)pyridine C6H3ClF3N (Mass of molecular ion: 181)
Source Temperature: 260 °C Sample Temperature: 160 °C Reservoir, 75 eV
26.0 1.2 28.0 2.4 31.0 2.3 37.0 1.4 38.0 1.5 49.0 2.2 50.0 8.8 51.0 5.8 52.0 1.9 57.0 2.2 60.0 1.6 62.0 1.0 63.5 1.1 68.0 1.0 69.0 15.9 70.0 1.1 75.0 14.5 76.0 7.2 77.0 2.6 81.0 1.2 85.0 2.5 87.0 1.0 95.0 1.0 96.0 3.5 99.0 3.1 100.0 1.8 112.0 1.1 119.0 6.1 120.0 1.0 126.0 32.6 127.0 2.9 131.0 1.1 146.0 95.6 147.0 6.7 162.0 11.8 164.0 4.1 181.0 100.0 182.0 7.1 183.0 32.2 184.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H3 Cl F3 N 0.042 g : 0.5 ml CDCl3 2-chloro-5-(trifluoromethyl)pyridine 
Assign. Shift(ppm)
A 8.689 B 7.904 C 7.497
Hz ppm Int.3473.88 8.693 736 3473.14 8.691 731 3472.29 8.689 736 3471.44 8.687 768 3465.70 8.672 34 3165.41 7.921 504 3164.79 7.919 525 3162.96 7.915 512 3162.35 7.913 514 3157.10 7.900 575 3156.49 7.899 599 3154.54 7.894 576 3153.93 7.892 576 3000.85 7.509 720 3000.24 7.508 1000 2999.51 7.506 772 2996.09 7.497 42 2992.55 7.488 652 2991.82 7.487 932 2991.09 7.485 691
in CDCl3
KBr disc
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