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MassMS-NW-6658 ethyl p-iodobenzoate C9H9IO2 (Mass of molecular ion: 276)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 4.2 29.0 7.2 37.0 1.0 38.0 1.5 39.0 1.5 45.0 3.8 50.0 20.7 51.0 3.2 65.0 6.6 73.0 1.6 74.0 8.0 75.0 9.0 76.0 35.5 77.0 4.9 93.0 1.1 103.0 3.2 104.0 9.7 105.0 2.0 121.0 3.2 127.0 1.6 149.0 6.8 203.0 21.1 204.0 1.8 231.0 100.0 232.0 12.1 248.0 44.0 249.0 3.9 276.0 54.2 277.0 5.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H9 I O2 0.05 ml : 0.5 ml CDCl3 ethyl p-iodobenzoate 
Assign. Shift(ppm)
A 7.75 B 4.355 C 1.378
Hz ppm Int.703.25 7.853 26 702.13 7.840 23 699.75 7.814 29 694.00 7.749 1000 688.00 7.683 31 685.63 7.656 26 684.44 7.643 28 401.13 4.479 76 393.88 4.398 251 386.81 4.320 262 379.75 4.241 87 130.38 1.456 278 128.31 1.433 29 123.31 1.377 566 119.38 1.333 26 116.13 1.297 245
in CDCl3
liquid film
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