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MS-NW-5074 N-methylbenzenesulfonamide C7H9NO2S (Mass of molecular ion: 171)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 1.7 28.0 4.8 30.0 32.2 39.0 2.4 50.0 6.7 51.0 22.0 52.0 1.6 65.0 1.6 66.0 1.1 74.0 2.0 75.0 1.8 76.0 2.0 77.0 100.0 78.0 18.7 79.0 2.1 94.0 4.8 106.0 8.6 107.0 5.9 110.0 1.2 125.0 1.3 141.0 17.8 142.0 3.3 143.0 1.3 171.0 22.1 172.0 2.1 173.0 1.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H9 N O2 S 0.04 ml : 0.5 ml CDCl3 N-methylbenzenesulfonamide Assign. Shift(ppm)
A 7.862 B 7.38 to 7.70 C 5.07 D 2.627
Hz ppm Int.
710.31 7.932 413 708.25 7.909 447 706.63 7.891 151 705.88 7.882 198 705.19 7.874 330 704.25 7.864 266 703.50 7.856 406 702.81 7.848 289 700.50 7.822 752 698.44 7.799 127 695.00 7.761 47 682.44 7.620 129 680.81 7.602 240 680.00 7.593 178 677.75 7.568 1000 675.81 7.546 871 673.00 7.515 361 672.38 7.508 321 671.94 7.503 280 671.38 7.497 279 670.56 7.488 450 667.44 7.453 107 665.88 7.436 145 663.31 7.407 50 661.44 7.386 54 452.88 5.057 60 235.25 2.627 888
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