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网站主页CAS数据库列表 5166-67-6更多图谱1-甲基-3-哌啶甲酸乙酯(5166-67-6)Raman光谱

1-甲基-3-哌啶甲酸乙酯

产品名称 1-甲基-3-哌啶甲酸乙酯

CAS号5166-67-6

分子式C9H17NO2

分子量171.24


  • Mass

    MS-NW-7601          
    ethyl 1-methyl-3-piperidinecarboxylate
    C9H17NO2            (Mass of molecular ion:    171)
    

       Source Temperature: 250 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       6.2
          17.0       1.0
          18.0       4.6
          26.0       3.7
          27.0      15.3
          28.0       7.9
          29.0      13.6
          30.0       4.9
          31.0       3.2
          39.0       8.1
          40.0       2.0
          41.0      10.8
          42.0      44.0
          43.0     100.0
          44.0      23.8
          45.0       2.4
          51.0       1.4
          52.0       1.6
          53.0       3.9
          54.0       5.0
          55.0      11.2
          56.0       6.9
          57.0      11.4
          58.0      23.8
          59.0       1.5
          65.0       1.4
          66.0       1.1
          67.0       2.3
          68.0       5.5
          69.0       3.1
          70.0      54.7
          71.0      36.2
          72.0       2.4
          73.0       6.4
          79.0       1.6
          80.0       1.5
          81.0       2.4
          82.0       7.7
          83.0       4.8
          84.0       8.9
          91.0       3.8
          92.0       3.3
          93.0       1.3
          94.0       3.7
          95.0       1.2
          96.0      18.8
          97.0      19.6
          98.0      56.9
          99.0       5.7
         101.0       5.7
         110.0       1.9
         112.0       1.2
         114.0       6.7
         124.0       5.9
         125.0       3.1
         126.0      37.5
         127.0       3.7
         128.0       1.4
         140.0       1.3
         142.0      88.7
         143.0      10.0
         144.0       1.0
         156.0       9.6
         157.0       1.1
         170.0      30.3
         171.0      46.1
         172.0       5.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H17 N O2 0.05 ml : 0.5 ml CDCl3
    ethyl 1-methyl-3-piperidinecarboxylate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.131 B 2.947 C 2.704 D 2.570 E 2.279 F 2.112 G 1.95 J 1.728 K 1.592 L 1.413 M 1.254

         Hz     ppm     Int.
    

       1662.35   4.160     78
       1661.50   4.158     85
       1655.15   4.142    214
       1654.42   4.140    230
       1647.95   4.124    220
       1647.22   4.122    235
       1640.75   4.106     81
       1640.14   4.104     84
       1177.73   2.947     36
       1168.58   2.925     37
       1086.79   2.720     36
       1075.81   2.692     37
       1037.84   2.597     49
       1033.94   2.588     30
       1031.25   2.581     39
       1030.76   2.580     40
       1026.86   2.570     72
       1022.95   2.560     39
       1020.26   2.553     34
       1016.48   2.544     56
        910.89   2.280   1000
        854.13   2.138     31
        843.63   2.111     56
        783.81   1.962     61
        781.49   1.956     76
        777.95   1.947     45
        772.95   1.935     49
        769.65   1.926     51
        764.77   1.914     38
        702.39   1.758     32
        698.49   1.748     39
        695.19   1.740     34
        688.96   1.724     53
        685.06   1.715     61
        681.88   1.707     46
        653.56   1.636     34
        645.75   1.616     31
        641.85   1.607     54
        640.14   1.602     30
        637.82   1.596     31
        630.62   1.578     43
        628.42   1.573     38
        569.95   1.427     32
        566.16   1.417     32
        557.13   1.395     30
        508.42   1.273    415
        501.22   1.255    723
        494.14   1.237    424
    

in CDCl3



liquid film