2-乙酰基-5-氯-3-甲基苯并[B]噻吩

产品名称 2-乙酰基-5-氯-3-甲基苯并[B]噻吩

CAS号51527-18-5

分子式C11H9ClOS

分子量224.71

¹³CNMR

Mass

MS-IW-2761          
2-acetyl-5-chloro-3-methylbenzo(b)thiophene
C11H9ClOS           (Mass of molecular ion:    224)

   Source Temperature: 190 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      31.0       1.0
      39.0       1.2
      43.0      10.4
      45.0       4.9
      50.0       1.2
      51.0       1.9
      62.0       1.2
      63.0       2.2
      69.0       5.0
      70.0       1.0
      72.0       1.1
      72.5       1.9
      73.0       2.7
      74.0       2.3
      75.0       3.4
      86.0       1.0
      87.0       1.7
      90.5       1.5
      93.0       1.7
      99.0       1.1
     101.0       4.3
     102.0       7.4
     103.0       1.0
     104.5       2.0
     112.0       2.0
     113.0       1.5
     115.0       1.5
     136.0       1.5
     137.0       1.8
     145.0      10.2
     146.0       7.9
     147.0       2.6
     149.0       2.7
     179.0       1.7
     180.0       1.0
     181.0      21.2
     182.0       2.7
     183.0       7.7
     209.0     100.0
     210.0      12.0
     211.0      36.7
     212.0       4.4
     213.0       1.7
     224.0      49.2
     225.0       6.6
     226.0      18.5
     227.0       2.4

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₁ H₉ Cl O S	0.039 g : 0.5 ml DMSO-d₆
2-acetyl-5-chloro-3-methylbenzo(b)thiophene

    Assign.     Shift(ppm)

      A             8.04
      B             8.03
      C             7.544
      D             2.667
      E             2.627

     Hz     ppm     Int.

   3213.75   8.042    154
   3211.30   8.036    227
   3202.64   8.014    157
   3202.15   8.013    158
   3020.51   7.558    106
   3018.43   7.553    104
   3011.84   7.537    100
   3009.77   7.532     99
   1066.04   2.668    890
   1052.98   2.635     43
   1050.17   2.628   1000

in DMSO-d6

KBr disc

nujol mull

更多供应商

2-乙酰基-5-氯-3-甲基苯并[B]噻吩(51527-18-5)质谱(MS) 相关产品图谱

2-乙酰-3-甲基苯并[B]噻吩(18781-31-2)核磁图(¹HNMR) 2-乙酰-3-甲基苯并[B]噻吩(18781-31-2)质谱(MS) 2-乙酰-3-甲基苯并[B]噻吩(18781-31-2)核磁图(¹³CNMR) 2-乙酰-3-甲基苯并[B]噻吩(18781-31-2)红外图谱(IR1) 2-乙酰-3-甲基苯并[B]噻吩(18781-31-2)红外图谱(IR2)

展开收起