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MS-NW-8643 2-(1-methyl-2-pyrrolidinyl)ethylamine C7H16N2 (Mass of molecular ion: 128)
Source Temperature: 260 °C Sample Temperature: 130 °C Reservoir, 75 eV
15.0 1.6 18.0 1.8 27.0 2.1 28.0 4.3 29.0 1.5 30.0 11.3 39.0 2.1 41.0 4.7 42.0 22.7 43.0 2.1 44.0 4.9 54.0 1.5 55.0 3.2 56.0 3.9 57.0 4.3 67.0 1.4 68.0 1.3 69.0 1.4 70.0 7.2 71.0 1.0 82.0 7.6 83.0 2.2 84.0 100.0 85.0 6.3 96.0 1.7 98.0 4.8 110.0 2.3 111.0 4.4 128.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H16 N2 0.05 ml : 0.5 ml CDCl3 2-(1-methyl-2-pyrrolidinyl)ethylamine Assign. Shift(ppm)
A 3.043 B *1 2.770 C *1 2.679 D 2.307 E 2.12 F 2.06 G *2 1.93 J 1.81 K *2 1.68 L *3 1.47 M *3 1.41
Hz ppm Int.
1226.07 3.068 52 1223.88 3.063 57 1216.55 3.045 96 1215.09 3.041 78 1208.98 3.026 55 1206.91 3.020 59 1116.70 2.795 46 1113.28 2.786 46 1110.11 2.778 76 1107.79 2.772 55 1104.49 2.764 77 1101.07 2.756 79 1095.46 2.742 74 1083.01 2.710 66 1076.66 2.695 74 1074.34 2.689 77 1070.80 2.680 44 1067.87 2.673 73 1062.13 2.658 45 922.00 2.308 1000 859.25 2.151 59 850.95 2.130 83 849.85 2.127 121 841.55 2.106 123 840.45 2.103 106 832.15 2.083 91 827.03 2.070 57 822.27 2.058 59 819.09 2.050 64 787.23 1.970 47 781.49 1.956 68 779.54 1.951 71 777.59 1.946 100 773.93 1.937 157 772.09 1.932 165 769.78 1.927 135 767.70 1.921 88 765.38 1.916 80 764.65 1.914 78 761.96 1.907 55 759.77 1.902 62 757.93 1.897 48 734.13 1.837 51 730.96 1.830 62 728.39 1.823 48 727.42 1.821 61 724.61 1.814 63 721.19 1.805 64 718.51 1.798 50 715.45 1.791 53 714.72 1.789 49 712.04 1.782 50 706.79 1.769 45 703.86 1.762 48 686.65 1.719 47 679.20 1.700 50 672.24 1.683 50 671.39 1.680 48 669.31 1.675 51 591.55 1.481 47 589.97 1.477 45 583.13 1.460 45 580.32 1.453 67 574.71 1.439 56 571.41 1.430 74 567.14 1.420 58 565.67 1.416 74 561.77 1.406 52 558.35 1.398 57 556.76 1.394 47 552.61 1.383 51
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