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网站主页CAS数据库列表 513-48-4更多图谱2-碘丁烷(513-48-4)质谱(MS)

2-碘丁烷

产品名称 2-碘丁烷

CAS号513-48-4

分子式C4H9I

分子量184.02

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  • Mass

    MS-NW-8320          
    2-iodobutane
    C4H9I               (Mass of molecular ion:    184)
    

       Source Temperature: 260 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          26.0       1.6
          27.0      12.7
          28.0       3.9
          29.0      53.9
          30.0       1.2
          39.0      11.1
          40.0       1.3
          41.0      46.8
          42.0       3.4
          43.0       1.0
          53.0       1.4
          55.0       4.4
          56.0       2.0
          57.0     100.0
          58.0       4.5
         127.0       3.9
         128.0       1.6
         184.0      11.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C4 H9 I 0.05 ml : 0.5 ml CDCl3
    2-iodobutane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.164 B 1.919 C *1 1.810 D *1 1.690 E 1.000

         Hz     ppm     Int.
    

       1681.03   4.207     31
       1676.03   4.194     38
       1674.19   4.190     90
       1673.10   4.187     44
       1669.19   4.177     97
       1667.36   4.173    106
       1666.14   4.169     99
       1662.35   4.160     99
       1661.13   4.157    107
       1659.30   4.152     95
       1655.40   4.143     41
       1654.30   4.140     92
       1652.47   4.135     36
       1647.46   4.123     30
        776.12   1.942     31
        775.76   1.942     31
        769.04   1.925   1000
        762.21   1.908    967
        739.87   1.852     69
        732.54   1.833    113
        725.34   1.815    150
        724.73   1.814    124
        718.02   1.797    139
        717.29   1.795    148
        709.96   1.777    115
        702.76   1.759     43
        694.34   1.738     41
        689.33   1.725     46
        687.13   1.720    113
        682.13   1.707    116
        680.05   1.702    135
        674.93   1.689    134
        672.85   1.684    101
        667.85   1.672     96
        665.41   1.665     72
        660.40   1.653     67
        658.33   1.648     30
        407.10   1.019    613
        399.90   1.001    946
        396.61   0.993     44
        392.58   0.983    550
    

in CDCl3



liquid film





REACTION WITH NA AT 77K