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MassMS-NW-1595 1-iodo-2-methylpropane C4H9I (Mass of molecular ion: 184)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.2 27.0 8.6 29.0 36.8 38.0 1.4 39.0 11.8 40.0 1.6 41.0 46.8 42.0 3.6 43.0 2.9 55.0 4.4 56.0 1.4 57.0 100.0 58.0 4.5 97.0 1.2 127.0 2.4 184.0 13.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C4 H9 I 0.05 ml : 0.5 ml CDCl3 1-iodo-2-methylpropane 
Assign. Shift(ppm)
A 3.139 B 1.74 C 1.02 J(A,B)=5.8HZ. J(B,C)=6.3HZ.
Hz ppm Int.284.31 3.175 463 278.50 3.110 521 167.63 1.872 25 162.75 1.818 25 161.56 1.804 37 160.81 1.796 21 156.88 1.752 21 155.69 1.739 50 154.56 1.726 43 149.69 1.672 29 148.69 1.661 52 142.69 1.594 44 93.50 1.044 1000 87.19 0.974 717
in CDCl3
CCl4 solution
liquid film
REACTION WITH NA AT 77K
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