-
MassMS-IW-4873 2-bromo-6-methoxynaphthalene C11H9BrO (Mass of molecular ion: 236)
Source Temperature: 130 °C Sample Temperature: 90 °C Direct, 75 eV
39.0 1.0 50.0 2.3 51.0 1.6 61.0 1.1 62.0 4.0 63.0 7.9 64.0 1.6 74.0 3.8 75.0 3.1 76.0 1.7 86.0 2.6 87.0 3.6 88.0 5.0 98.0 1.3 99.0 1.4 113.0 9.4 114.0 26.2 115.0 2.7 118.0 3.3 119.0 3.3 126.0 9.1 127.0 4.6 128.0 2.9 142.0 2.5 156.0 1.1 157.0 1.9 193.0 41.1 194.0 4.6 195.0 40.1 196.0 3.9 206.0 2.0 207.0 1.2 208.0 1.9 221.0 15.3 222.0 2.0 223.0 15.1 224.0 1.7 236.0 100.0 237.0 12.4 238.0 98.3 239.0 11.9
400 MHz in CDCl3
-
1H NMR 399.65 MHz C11 H9 Br O 0.039 g : 0.5 ml CDCl3 2-bromo-6-methoxynaphthalene 
Assign. Shift(ppm)
A 7.891 B 7.612 C 7.571 D 7.482 E 7.144 F 7.066 G 3.886
Hz ppm Int.3154.79 7.894 126 3153.08 7.890 125 3047.00 7.625 111 3037.84 7.602 123 3031.25 7.585 93 3022.46 7.563 143 2994.51 7.493 126 2992.55 7.488 119 2985.84 7.472 80 2983.76 7.466 78 2860.84 7.159 95 2858.28 7.152 107 2851.81 7.136 86 2849.24 7.130 99 2825.07 7.069 126 2822.63 7.063 108 1553.34 3.887 1000
in CDCl3
KBr disc
nujol mull
更多供应商
