氯解磷定

Mass

MS-NW-8736          
2-hydroxyiminomethyl-1-methylpyridinium chloride
C6H6N2O CH3Cl       (Mass of molecular ion:    172)

   Source Temperature: 230 °C
   Sample Temperature: 170 °C
   Direct, 75 eV

      15.0       4.3
      17.0       5.5
      18.0      29.2
      26.0       5.8
      27.0      26.9
      28.0       7.4
      30.0       1.1
      35.0       6.2
      36.0      82.0
      37.0       3.9
      38.0      28.3
      39.0      12.1
      40.0       2.9
      41.0       5.4
      42.0       8.5
      43.0       1.3
      44.0       1.6
      49.0       2.2
      50.0      17.1
      51.0      20.4
      52.0      15.0
      53.0       6.9
      54.0       2.1
      55.0       1.8
      59.0       1.1
      59.5       1.7
      61.0       1.3
      62.0       2.2
      63.0       6.9
      64.0       9.8
      65.0      18.4
      66.0       8.2
      67.0       3.7
      68.0       1.4
      75.0       3.5
      76.0       8.4
      77.0      38.2
      78.0      74.5
      79.0      21.2
      80.0       7.0
      81.0       6.1
      90.0       4.9
      91.0       8.2
      92.0      28.9
      93.0      10.4
      94.0       3.2
     103.0       6.0
     104.0      65.0
     105.0       8.2
     106.0       5.7
     107.0      10.5
     108.0       2.4
     109.0      17.9
     110.0       1.5
     117.0       4.2
     118.0      42.2
     119.0     100.0
     120.0      13.8
     121.0       3.7
     122.0       7.3
     129.0       1.0
     131.0       2.1
     132.0       6.6
     133.0       1.0
     135.0       6.0
     136.0      38.9
     137.0       6.4
     138.0       2.1
     144.0       1.9
     193.0       1.1
     194.0       1.4
     195.0       1.2
     208.0       2.5
     209.0       1.6

Assign. Shift(ppm) A 8.818 B 8.730 C 8.543 D 8.427 E 8.039 F 4.444

     Hz     ppm     Int.

   3527.83   8.828    111
   3527.34   8.827    109
   3521.61   8.812    116
   3521.00   8.811    114
   3489.01   8.731    390
   3423.46   8.567     47
   3422.97   8.565     48
   3415.28   8.546    113
   3407.59   8.527     71
   3407.10   8.526     72
   3372.19   8.438    111
   3370.97   8.435    124
   3364.01   8.418     83
   3362.79   8.415     88
   3220.70   8.059     56
   3219.24   8.056     60
   3214.36   8.043     64
   3213.01   8.040    107
   3206.67   8.024     52
   3205.32   8.021     54
   1776.00   4.444   1000