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MS-IW-9115 1-chloroethyl ethyl carbonate C5H9ClO3 (Mass of molecular ion: 152)
Source Temperature: 200 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 2.6 19.0 1.1 26.0 3.1 27.0 21.7 28.0 8.9 29.0 48.8 30.0 1.7 31.0 3.5 36.0 2.1 43.0 18.6 44.0 11.7 45.0 100.0 46.0 2.5 62.0 4.5 63.0 30.4 64.0 3.6 65.0 10.4 73.0 2.1 74.0 1.5 79.0 3.0 81.0 1.0 90.0 3.2 91.0 2.6 117.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C5 H9 Cl O3 0.05 ml : 0.5 ml CDCl3 1-chloroethyl ethyl carbonate Assign. Shift(ppm)
A 6.441 B 4.273 C 1.833 D 1.343
Hz ppm Int.
2583.01 6.464 118 2577.15 6.449 330 2571.29 6.434 329 2565.55 6.420 115 1718.87 4.301 163 1715.21 4.292 29 1711.79 4.284 456 1708.86 4.276 23 1708.13 4.275 27 1704.59 4.266 481 1700.81 4.256 22 1697.39 4.248 192 742.43 1.858 20 735.47 1.841 1000 729.61 1.826 962 544.07 1.362 612 541.26 1.355 39 536.87 1.344 989 529.54 1.326 587
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