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MassMS-NW-6484 (2,6-dichlorophenyl)hydrazine hydrochloride C6H6Cl2N2 HCl (Mass of molecular ion: 176)
Source Temperature: 110 °C Sample Temperature: 90 °C Direct, 75 eV
16.0 1.4 17.0 1.9 18.0 10.4 28.0 4.5 29.0 4.2 30.0 1.6 31.0 4.3 35.0 5.8 36.0 59.6 37.0 4.2 38.0 19.3 39.0 2.5 44.5 1.8 47.0 1.3 49.0 2.2 50.0 6.0 51.0 7.9 52.0 7.3 61.0 3.2 62.0 5.0 63.0 7.4 64.0 2.1 72.0 1.8 73.0 7.4 74.0 7.4 75.0 16.8 76.0 11.6 77.0 7.1 78.0 4.4 83.0 1.0 84.0 2.7 85.0 2.7 86.0 1.7 87.0 1.6 88.0 3.1 89.0 1.8 90.0 3.4 97.0 2.2 98.0 2.1 99.0 3.3 101.0 1.0 105.0 1.6 107.0 1.1 109.0 2.5 110.0 2.2 111.0 14.4 112.0 3.9 113.0 5.2 114.0 3.3 124.0 11.7 125.0 7.4 126.0 5.0 127.0 2.6 133.0 27.4 134.0 1.7 135.0 18.6 136.0 1.1 137.0 3.0 139.0 1.3 141.0 6.5 143.0 2.0 146.0 8.0 147.0 1.4 148.0 5.6 159.0 4.5 160.0 59.5 161.0 24.2 162.0 39.1 163.0 14.2 164.0 7.3 165.0 2.4 175.0 1.7 176.0 100.0 177.0 8.3 178.0 64.3 179.0 5.0 180.0 11.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H6 Cl2 N2 0.040 g : 0.5 ml DMSO-d6 (2,6-dichlorophenyl)hydrazine hydrochloride 
Assign. Shift(ppm)
A 10.4 B 7.537 C 7.292 D 7.23
Hz ppm Int.4147.25 10.378 110 3016.94 7.549 820 3013.64 7.541 28 3012.17 7.538 33 3008.88 7.529 1000 2921.87 7.312 303 2914.18 7.292 375 2913.45 7.291 312 2905.75 7.271 234 2890.55 7.233 102
in DMSO-d6
KBr disc
nujol mull
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