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MassMS-IW-1286 ethyl 4-indolecarboxylate C11H11NO2 (Mass of molecular ion: 189)
Source Temperature: 130 °C Sample Temperature: 90 °C Direct, 75 eV
27.0 1.4 28.0 1.2 29.0 1.4 39.0 1.5 58.0 1.5 62.0 2.1 63.0 3.6 72.0 1.6 88.0 1.5 89.0 8.7 90.0 2.0 114.0 1.2 115.0 3.6 116.0 28.0 117.0 19.2 118.0 1.8 143.0 1.3 144.0 79.3 145.0 10.8 161.0 18.5 162.0 1.9 174.0 5.2 175.0 1.1 188.0 1.5 189.0 100.0 190.0 12.6 191.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H11 N O2 0.036 g : 0.5 ml CDCl3 ethyl 4-indolecarboxylate 
Assign. Shift(ppm)
A 8.66 B 7.939 C 7.561 D 7.313 E 7.220 F 7.193 G 4.461 J 1.454
Hz ppm Int.3177.37 7.951 199 3176.39 7.948 207 3169.92 7.932 210 3168.95 7.930 209 3026.98 7.575 110 3026.00 7.572 197 3025.02 7.570 110 3018.92 7.554 129 3017.94 7.552 225 3016.97 7.550 124 2925.66 7.321 121 2922.61 7.313 165 2920.04 7.307 133 2893.19 7.240 143 2885.62 7.221 201 2877.93 7.202 184 2877.56 7.201 185 2876.10 7.197 134 2875.12 7.195 191 2874.02 7.192 112 2872.92 7.189 106 2871.95 7.187 98 1793.70 4.489 159 1786.62 4.471 480 1779.42 4.453 518 1772.34 4.435 168 588.50 1.473 527 581.42 1.455 1000 578.86 1.449 35 574.22 1.437 521
in CDCl3
KBr disc
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