图谱信息 供应商 相关产品
网站主页CAS数据库列表 50585-29-0更多图谱1,8-BIS(CHLOROMETHYL)NAPHTHALENE(50585-29-0)核磁图(13CNMR)

1,8-BIS(CHLOROMETHYL)NAPHTHALENE

产品名称 1,8-BIS(CHLOROMETHYL)NAPHTHALENE

CAS号50585-29-0

分子式C12H10Cl2

分子量225.11

展开


  • Mass

    MS-IW-0633          
    1,8-bis(chloromethyl)naphthalene
    C12H10Cl2           (Mass of molecular ion:    224)
    

       Source Temperature: 140 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          36.0       2.1
          50.0       1.2
          51.0       2.3
          62.0       1.2
          63.0       7.1
          64.0       2.7
          74.0       1.3
          75.0       4.2
          75.5       5.1
          76.0      26.8
          76.5       9.9
          77.0       4.6
          94.0       1.5
         115.0       1.3
         126.0       1.7
         127.0       1.7
         139.0       1.8
         141.0       3.1
         142.0       1.6
         150.0       3.3
         151.0       8.1
         152.0      27.0
         153.0      36.4
         154.0      15.3
         155.0       3.2
         169.0       1.4
         170.0       3.5
         187.0       8.4
         188.0       1.7
         189.0     100.0
         190.0      13.9
         191.0      32.3
         192.0       4.5
         224.0      31.9
         225.0       4.5
         226.0      21.0
         227.0       2.8
         228.0       3.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H10 Cl2 0.022 g : 0.5 ml CDCl3
    1,8-bis(chloromethyl)naphthalene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.897 B 7.602 C 7.464 D 5.324

         Hz     ppm     Int.
    

       3161.13   7.910    129
       3159.79   7.907    141
       3152.83   7.889    144
       3151.49   7.886    156
       3042.97   7.615    123
       3041.50   7.611    126
       3035.89   7.597    155
       3034.42   7.593    165
       2990.23   7.483    154
       2983.15   7.465    142
       2982.06   7.462    174
       2974.98   7.444    113
       2128.05   5.325   1000
    

in CDCl3