400 MHz in CDCl3
-
1H NMR 399.65 MHz C25 H28 O3 0.039 g : 0.5 ml CDCl3 estradiol-17beta 3-benzoate 
Assign. Shift(ppm)
A 8.194 B 7.617 C 7.499 D 7.334 E 6.924 F 6.972 G 3.726 J 2.89 K 2.342 L 2.243 M *1 2.113 N 1.960 P 1.893 Q *2 1.703 R 0.78 S 1.53 T *1 1.48 U *2 1.37 V 1.32 W 1.198 X 0.783 ASSIGNED BY C-H AND H-H COSY.
Hz ppm Int.3281.25 8.211 43 3279.54 8.207 213 3278.93 8.205 195 3278.20 8.203 260 3273.07 8.190 81 3271.12 8.185 284 3269.78 8.182 245 3054.44 7.643 35 3053.10 7.640 64 3051.76 7.637 39 3047.61 7.626 49 3045.65 7.621 153 3043.82 7.617 54 3039.55 7.606 68 3038.21 7.603 115 3036.87 7.599 60 3004.03 7.517 192 3002.44 7.513 86 2996.09 7.497 281 2990.36 7.483 58 2988.65 7.479 137 2935.67 7.346 115 2927.49 7.326 130 2791.99 6.987 85 2789.43 6.980 101 2783.45 6.965 75 2781.01 6.959 96 2768.55 6.928 183 2765.99 6.922 142 1489.38 3.727 60 1157.59 2.897 98 1151.00 2.881 91 1147.46 2.872 105 944.09 2.363 40 941.04 2.355 44 930.54 2.329 45 927.61 2.322 46 898.56 2.249 48 896.00 2.242 39 894.65 2.239 40 855.10 2.140 35 849.73 2.127 41 845.58 2.116 46 841.92 2.107 45 840.45 2.103 35 836.43 2.093 43 793.95 1.987 38 790.41 1.978 58 787.48 1.971 42 781.37 1.956 47 778.44 1.948 63 777.95 1.947 63 774.90 1.939 41 765.14 1.915 38 762.82 1.909 40 760.62 1.904 36 753.17 1.885 47 750.49 1.878 49 747.56 1.871 41 689.45 1.726 42 686.89 1.719 41 684.57 1.713 42 677.12 1.695 44 674.68 1.689 43 634.16 1.587 128 624.51 1.563 54 620.61 1.553 47 612.55 1.533 58 611.21 1.530 54 608.76 1.524 67 602.05 1.507 57 598.51 1.498 90 595.58 1.491 76 593.99 1.487 62 592.29 1.483 40 590.33 1.478 50 586.55 1.468 78 585.45 1.465 77 580.44 1.453 37 577.39 1.445 42 576.17 1.442 42 562.26 1.407 51 556.03 1.392 68 554.44 1.388 58 550.42 1.378 90 544.07 1.362 91 542.60 1.358 71 538.45 1.348 86 531.98 1.332 87 527.34 1.320 58 519.41 1.300 69 515.14 1.289 58 492.92 1.234 51 485.60 1.216 50 481.93 1.206 51 480.83 1.204 53 474.37 1.187 53 313.23 0.784 1000
in CDCl3
KBr disc
4880 A,200 M,powder
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