400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H16 O7 0.041 g : 0.5 ml DMSO-d6 p-hydroxyphenyl beta-D-glucopyranoside 
Assign. Shift(ppm)
A 9.01 B 6.870 C 6.667 D *1 5.25 E *1 5.05 F *1 4.99 G 4.649 J 4.56 K *2 3.688 L *2 3.460 M 3.24 N 3.19 P 3.15 ASSIGNED BY C-H COSY
Hz ppm Int.3602.29 9.014 940 2754.52 6.893 71 2750.85 6.884 775 2748.54 6.878 267 2744.14 6.867 297 2741.82 6.861 1000 2738.16 6.852 107 2672.12 6.687 108 2668.58 6.678 992 2666.26 6.672 306 2661.87 6.661 276 2659.55 6.655 839 2655.76 6.646 76 2101.81 5.260 498 2096.80 5.247 523 2022.83 5.062 430 2018.19 5.050 433 1996.34 4.996 461 1991.21 4.983 476 1862.06 4.660 462 1854.61 4.641 480 1828.49 4.576 194 1822.51 4.561 358 1816.89 4.547 204 1484.01 3.714 88 1482.42 3.710 100 1478.76 3.701 97 1477.05 3.696 109 1472.41 3.685 135 1470.58 3.680 130 1467.04 3.671 127 1465.45 3.667 119 1396.36 3.494 86 1390.38 3.479 171 1384.40 3.465 183 1378.66 3.450 144 1372.56 3.435 105 1305.54 3.267 116 1303.59 3.262 123 1302.25 3.259 111 1297.97 3.248 248 1296.02 3.243 218 1293.58 3.237 288 1289.55 3.227 289 1284.79 3.215 216 1281.74 3.208 171 1276.86 3.195 169 1274.29 3.189 181 1269.17 3.176 187 1266.97 3.171 213 1261.47 3.157 184 1258.06 3.148 144 1252.81 3.135 132 1252.44 3.134 132 1248.90 3.125 75 1243.65 3.112 69
in D2O
in DMSO-d6
KBr disc
nujol mull
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