乙醇药用

Mass

MS-NW-8769          
endo-norborneol
C7H12O              (Mass of molecular ion:    112)

   Source Temperature: 280 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.1
      27.0      13.2
      28.0       3.3
      29.0      12.7
      31.0       4.2
      38.0       1.2
      39.0      20.2
      40.0       6.3
      41.0      31.8
      42.0       7.2
      43.0      12.2
      44.0       6.4
      45.0       7.3
      50.0       1.1
      51.0       2.9
      52.0       1.4
      53.0      14.5
      54.0       6.0
      55.0      25.6
      56.0      12.4
      57.0      35.0
      58.0       5.0
      65.0       6.0
      66.0      61.2
      67.0      95.6
      68.0      74.8
      69.0      10.2
      70.0      15.3
      71.0       7.1
      77.0       7.2
      78.0       2.4
      79.0     100.0
      80.0       7.6
      81.0      15.8
      82.0       2.1
      83.0      20.6
      84.0       5.3
      91.0       2.8
      93.0       7.2
      94.0      91.2
      95.0      12.6
      97.0       6.4
     111.0       1.5
     112.0       1.5

Assign. Shift(ppm) A 4.216 B 2.24 C 2.16 D 2.07 E 1.94 F 1.88 G 1.56 J 1.37 K 1.34 L 1.30 M 1.29 N 0.843 ASSIGNED BY H-H AND C-H COSY.

     Hz     ppm     Int.

   1694.21   4.240    162
   1692.99   4.237    179
   1689.82   4.229    286
   1686.52   4.220    193
   1684.69   4.216    230
   1682.86   4.211    196
   1679.69   4.203    285
   1676.27   4.195    167
   1674.93   4.191    155
    900.02   2.253    302
    895.75   2.242    529
    891.60   2.231    288
    868.41   2.173    269
    864.26   2.163    493
    859.62   2.151    295
    852.54   2.134     46
    852.17   2.133     44
    850.34   2.128     37
    826.54   2.069    702
    789.31   1.976    205
    786.25   1.968    235
    784.42   1.963    206
    781.37   1.956    215
    779.05   1.950    219
    776.12   1.942    383
    774.17   1.938    250
    773.32   1.935    297
    771.36   1.931    356
    768.55   1.924    239
    765.99   1.917    328
    763.06   1.910    392
    761.23   1.905    280
    759.89   1.902    142
    758.30   1.898    240
    756.71   1.894    198
    754.27   1.888    227
    753.30   1.885    230
    751.46   1.881    259
    749.88   1.877    249
    749.51   1.876    249
    746.83   1.869    165
    744.26   1.863    197
    742.07   1.857    193
    738.04   1.847    111
    735.84   1.842    155
    642.70   1.609     58
    639.40   1.600     71
    638.79   1.599     76
    636.60   1.593    101
    635.74   1.591     87
    633.54   1.586    111
    632.32   1.583    108
    629.52   1.576    226
    625.24   1.565    322
    622.07   1.557    298
    617.19   1.545    174
    613.53   1.536    223
    610.35   1.528    155
    609.25   1.525    210
    606.08   1.517    116
    564.58   1.413     40
    561.28   1.405     50
    558.72   1.399    155
    557.25   1.395    167
    554.44   1.388    275
    552.98   1.384    284
    549.68   1.376    233
    547.97   1.372    334
    546.02   1.367    500
    544.56   1.363    389
    542.24   1.357    482
    540.65   1.353    465
    537.72   1.346    736
    536.01   1.342   1000
    534.06   1.337    682
    532.59   1.333    431
    529.17   1.325    388
    527.34   1.320    505
    525.15   1.315    345
    523.07   1.309    309
    520.63   1.303    193
    519.17   1.300    369
    517.58   1.296    636
    515.87   1.291    660
    514.04   1.287    637
    512.33   1.282    365
    509.40   1.275    174
    507.69   1.271    277
    505.98   1.267    285
    504.27   1.262    286
    502.56   1.258    158
    346.44   0.867    338
    343.02   0.859    593
    339.60   0.850    311
    333.62   0.835    317
    330.08   0.826    548
    326.66   0.818    282