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MassMS-IW-9006 7-chloro-2- methylquinoline C10H8ClN (Mass of molecular ion: 177)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
38.0 1.1 39.0 3.2 50.0 3.8 51.0 3.7 52.0 1.0 57.5 1.4 61.0 1.1 62.0 2.2 63.0 4.1 64.0 1.0 68.0 1.3 70.5 3.6 73.0 1.3 74.0 4.0 75.0 6.2 75.5 2.2 76.0 1.9 86.0 1.1 87.0 1.6 88.0 1.6 88.5 2.6 89.0 3.2 98.0 1.0 99.0 4.1 100.0 2.2 101.0 2.3 102.0 1.2 110.0 1.0 113.0 2.5 114.0 3.4 115.0 15.2 116.0 3.8 126.0 3.0 127.0 3.7 135.0 1.6 136.0 1.1 140.0 5.8 141.0 4.5 142.0 15.9 143.0 1.8 149.0 2.1 150.0 1.0 151.0 1.9 162.0 9.1 163.0 1.1 164.0 3.0 176.0 3.5 177.0 100.0 178.0 12.4 179.0 32.3 180.0 3.7 191.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H8 Cl N 0.040 g : 0.5 ml CDCl3 7-chloro-2- methylquinoline 
Assign. Shift(ppm)
A 8.002 B 7.982 C 7.665 D 7.407 E 7.252 F 2.720
Hz ppm Int.3199.22 8.006 147 3197.27 8.001 156 3194.21 7.993 141 3185.67 7.972 131 3067.99 7.677 143 3059.33 7.656 169 2965.33 7.420 110 2963.26 7.415 110 2956.67 7.399 95 2954.59 7.393 93 2902.71 7.264 188 2894.29 7.243 180 1087.28 2.721 1000
in CDCl3
KBr disc
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