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MassMS-NW-7926 2-amino-4-methylbenzophenone C14H13NO (Mass of molecular ion: 211)
Source Temperature: 160 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 1.1 27.0 1.4 28.0 1.8 39.0 2.8 50.0 1.7 51.0 6.7 52.0 2.2 53.0 1.8 63.0 1.6 65.0 1.4 66.0 1.1 76.0 1.5 77.0 25.8 78.0 3.8 79.0 8.7 80.0 1.0 83.5 1.2 89.0 1.2 90.0 1.1 90.5 2.8 91.0 1.3 91.5 1.2 104.0 2.6 104.5 5.5 105.0 9.2 105.5 1.6 106.0 13.8 107.0 1.3 115.0 1.0 134.0 41.8 135.0 4.0 165.0 1.2 166.0 1.1 167.0 3.1 168.0 1.0 180.0 2.5 181.0 1.3 182.0 4.0 183.0 1.0 194.0 6.0 195.0 3.5 196.0 1.4 209.0 1.7 210.0 100.0 211.0 77.1 212.0 11.2 213.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H13 N O 0.050 g : 0.5 ml CDCl3 2-amino-4-methylbenzophenone 
Assign. Shift(ppm)
A 7.604 B 7.487 C 7.433 D 7.329 E 6.522 F 6.401 G 6.13 J 2.267
Hz ppm Int.3046.51 7.623 33 3044.43 7.618 204 3043.09 7.615 257 3041.50 7.611 130 3038.45 7.603 87 3036.25 7.598 354 3034.79 7.594 273 3002.08 7.512 54 3000.61 7.509 32 2997.44 7.501 38 2994.75 7.494 170 2992.31 7.488 53 2988.89 7.479 101 2987.43 7.476 161 2985.96 7.472 76 2978.03 7.452 61 2976.81 7.449 202 2976.07 7.447 261 2974.73 7.444 107 2970.21 7.433 195 2968.63 7.429 300 2966.92 7.424 75 2963.26 7.415 54 2961.67 7.411 132 2960.33 7.408 72 2933.47 7.341 222 2925.29 7.320 232 2606.69 6.523 215 2562.87 6.413 121 2562.50 6.412 120 2561.28 6.409 116 2554.69 6.393 115 2554.32 6.392 116 2553.10 6.389 112 2451.29 6.134 95 906.01 2.268 1000
in CDCl3
KBr disc
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