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MS-NW-2221 cis-decahydronaphthalene C10H18 (Mass of molecular ion: 138)
Source Temperature: 280 °C Sample Temperature: 170 °C Reservoir, 75 eV
18.0 1.0 27.0 12.8 28.0 1.0 29.0 11.1 39.0 18.5 40.0 3.2 41.0 43.8 42.0 3.8 43.0 3.9 51.0 2.7 52.0 1.6 53.0 10.9 54.0 19.2 55.0 34.1 56.0 3.2 57.0 1.1 65.0 3.3 66.0 6.4 67.0 90.8 68.0 36.5 69.0 18.7 70.0 2.4 77.0 4.3 78.0 1.2 79.0 8.8 80.0 6.3 81.0 86.3 82.0 69.5 83.0 11.7 91.0 2.2 93.0 2.8 94.0 3.0 95.0 50.8 96.0 100.0 97.0 11.0 108.0 1.1 109.0 32.4 110.0 9.3 123.0 1.2 138.0 84.8 139.0 9.4
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C10 H18 0.04 ml : 0.5 ml CDCl3 cis-decahydronaphthalene Assign. Shift(ppm)
A 1.62 B 1.82 to 1.07
Hz ppm Int.
162.31 1.813 26 161.63 1.805 29 159.06 1.777 50 158.06 1.765 62 156.94 1.753 72 144.50 1.614 529 139.13 1.554 377 133.75 1.494 687 133.25 1.488 690 128.31 1.433 998 127.81 1.428 1000 126.94 1.418 993 126.50 1.413 995 126.19 1.409 993 115.63 1.292 302 114.88 1.283 307 101.88 1.138 46 100.19 1.119 34 99.63 1.113 28
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1H NMR 399.65 MHz C10 H18 0.023 g : 0.5 ml CDCl3 cis-decahydronaphthalene Assign. Shift(ppm)
A 1.65 B *1 1.52 C *1 1.31 ASSIGNED BY C-H COSY.
Hz ppm Int.
685.42 1.716 27 660.40 1.653 567 610.96 1.529 1000 523.32 1.310 989
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