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MassMS-NW-3763 4-methylquinoline C10H9N (Mass of molecular ion: 143)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
39.0 3.5 50.0 2.5 51.0 3.4 57.5 1.6 58.5 1.7 62.0 1.6 63.0 3.8 64.0 1.2 65.0 1.7 70.5 1.2 71.5 1.5 74.0 1.5 75.0 2.5 76.0 1.6 77.0 3.6 88.0 1.0 89.0 4.4 90.0 2.1 101.0 1.8 102.0 1.1 104.0 3.4 114.0 1.4 115.0 19.5 116.0 7.1 117.0 4.2 128.0 2.3 140.0 1.3 141.0 1.4 142.0 15.9 143.0 100.0 144.0 11.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H9 N 22.9 mg : 0.5 ml CDCl3 4-methylquinoline 
Assign. Shift(ppm)
A 8.775 B 8.110 C 7.985 D 7.705 E 7.559 F 7.215 G 2.691 J(A,F)=4.4HZ J(F,G)=-0.9HZ
Hz ppm Int.3509.16 8.781 196 3504.76 8.770 203 3246.34 8.123 116 3245.61 8.122 119 3245.12 8.120 113 3238.40 8.104 110 3237.79 8.102 130 3237.18 8.101 132 3236.57 8.099 125 3196.41 7.999 97 3195.92 7.997 109 3195.07 7.995 115 3194.58 7.994 111 3187.99 7.977 110 3187.50 7.976 121 3186.65 7.974 128 3186.16 7.973 124 3087.89 7.727 80 3086.43 7.723 85 3081.05 7.710 104 3079.59 7.706 162 3078.00 7.702 88 3072.63 7.689 96 3071.17 7.685 96 3028.93 7.579 97 3027.71 7.576 104 3022.09 7.562 84 3020.63 7.559 158 3019.29 7.555 105 3013.67 7.541 77 3012.45 7.538 78 2886.84 7.224 128 2885.99 7.222 139 2882.57 7.213 137 2881.59 7.211 143 1075.93 2.693 937 1074.95 2.690 1000
in CDCl3
liquid film
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