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MassMS-NW-6925 1-amino-1-deoxy-D-glucitol C6H15NO5 (Mass of molecular ion: 181)
Source Temperature: 210 °C Sample Temperature: 140 °C Direct, 75 eV
15.0 11.1 18.0 10.2 19.0 6.1 26.0 1.0 27.0 5.9 28.0 7.5 29.0 9.6 30.0 100.0 31.0 15.5 32.0 1.9 39.0 1.8 41.0 3.8 42.0 10.6 43.0 16.7 44.0 8.0 45.0 7.6 48.0 1.6 55.0 3.0 56.0 3.2 57.0 5.2 59.0 1.7 60.0 22.3 61.0 8.0 69.0 1.7 71.0 2.6 72.0 4.2 73.0 27.3 74.0 2.0 85.0 1.3 86.0 1.1 90.0 5.9 91.0 1.7 102.0 7.9 103.0 2.0 116.0 1.7 120.0 3.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H15 N O5 0.039 g : 0.5 ml DMSO-d6 1-amino-1-deoxy-D-glucitol 
Assign. Shift(ppm)
A 3.64 B *1 3.59 C 3.53 D 3.50 E 3.427 F *1 3.409 G *2 2.685 J *2 2.604
Hz ppm Int.1457.40 3.647 886 1455.69 3.643 934 1452.64 3.635 1000 1450.93 3.631 972 1443.24 3.612 727 1439.45 3.602 676 1432.50 3.585 587 1428.83 3.576 610 1415.77 3.543 288 1410.64 3.530 481 1405.27 3.517 543 1403.56 3.512 392 1401.37 3.507 421 1397.83 3.498 311 1395.75 3.493 371 1391.97 3.483 318 1374.02 3.439 520 1372.19 3.434 513 1368.29 3.424 550 1366.33 3.419 422 1364.50 3.415 401 1362.55 3.410 414 1357.54 3.397 382 1351.81 3.383 292 1083.50 2.712 109 1079.10 2.701 118 1071.04 2.680 216 1066.53 2.669 209 1047.97 2.623 233 1042.36 2.609 234 1035.28 2.591 139 1029.66 2.577 125
in D2O
in DMSO-d6
KBr disc
nujol mull
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