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2-甲基-3-硝基苯甲醚

产品名称 2-甲基-3-硝基苯甲醚

CAS号4837-88-1

分子式C8H9NO3

分子量167.16

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  • Mass

    MS-IW-0564          
    2-methyl-3-nitroanisole
    C8H9NO3             (Mass of molecular ion:    167)
    

       Source Temperature: 260 °C
       Sample Temperature: 130 °C
       Reservoir, 75 eV
    

          15.0       1.0
          27.0       2.2
          28.0       2.6
          30.0       1.1
          38.0       1.5
          39.0      11.4
          40.0       1.2
          41.0       2.9
          43.0       2.0
          50.0       5.9
          51.0      19.3
          52.0      15.3
          53.0       5.3
          55.0       1.6
          59.0       1.4
          62.0       2.3
          63.0       9.6
          64.0       3.9
          65.0      29.9
          66.0       5.0
          67.0       2.0
          74.0       1.4
          75.0       1.9
          76.0       3.5
          77.0      31.0
          78.0      30.2
          79.0       8.6
          80.0       1.5
          89.0       7.1
          90.0      14.8
          91.0      56.6
          92.0     100.0
          93.0       9.7
          94.0       4.6
          95.0       7.2
         105.0      17.4
         106.0      16.0
         107.0       7.7
         108.0       2.1
         120.0       1.9
         121.0       1.6
         122.0       5.8
         135.0       7.9
         150.0      77.6
         151.0       7.7
         167.0      52.0
         168.0       5.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H9 N O3 0.038 g : 0.5 ml CDCl3
    2-methyl-3-nitroanisole
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.383 B 7.259 C 7.042 D 3.885 E 2.349

         Hz     ppm     Int.
    

       2955.32   7.395     81
       2954.22   7.393     86
       2947.14   7.375    114
       2946.04   7.372    118
       2909.55   7.281     65
       2909.06   7.280     75
       2901.37   7.260    117
       2900.76   7.259    137
       2893.07   7.240     57
       2892.58   7.238     67
       2818.12   7.052    104
       2817.75   7.051    104
       2810.30   7.032     84
       2809.94   7.032     87
       2809.57   7.031     86
       1552.61   3.885   1000
        938.72   2.349    763
    

in CDCl3



KBr disk



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