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N,N'-二正丁基-1,6-己二胺

产品名称 N,N'-二正丁基-1,6-己二胺

CAS号4835-11-4

分子式C14H32N2

分子量228.42

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  • Mass

    MS-NW-3935          
    N,N'-dibutyl-1,6-hexanediamine
    C14H32N2            (Mass of molecular ion:    228)
    

       Source Temperature: 280 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          18.0       1.4
          27.0       3.6
          28.0       4.6
          29.0      12.8
          30.0      32.0
          39.0       2.5
          41.0      15.8
          42.0       5.8
          43.0       5.7
          44.0      25.7
          45.0       1.0
          53.0       1.0
          55.0      10.7
          56.0       7.6
          57.0       8.6
          58.0       2.8
          68.0       1.3
          69.0       1.7
          70.0       5.7
          71.0       9.4
          72.0       8.6
          73.0       5.9
          74.0       2.7
          81.0       3.9
          82.0       1.4
          83.0       1.2
          84.0       5.2
          86.0     100.0
          87.0       6.2
          96.0       1.0
          98.0      15.6
          99.0       2.4
         100.0      22.8
         101.0       2.0
         110.0       3.8
         112.0      42.9
         113.0       3.8
         114.0       8.6
         126.0       2.4
         128.0       2.4
         140.0       1.3
         142.0      15.1
         143.0       6.3
         154.0      19.9
         155.0       3.2
         156.0      10.6
         157.0       2.8
         171.0       5.1
         185.0      16.3
         186.0       2.3
         228.0       1.9
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C14 H32 N2 0.04 ml : 0.5 ml CDCl3
    N,N'-dibutyl-1,6-hexanediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.59 B 1.66 C 1.49 D 1.47 E 1.35 F 1.33 G 0.915

         Hz     ppm     Int.
    

        239.06   2.670    359
        232.19   2.593    903
        225.31   2.516    590
        148.50   1.659     34
        147.56   1.648     42
        146.94   1.641     43
        145.00   1.620     76
        144.56   1.615     75
        139.31   1.556    199
        137.13   1.532    231
        131.50   1.469    491
        128.44   1.435    607
        127.25   1.421    684
        123.81   1.383    997
        115.00   1.285    233
        109.69   1.225    145
        109.13   1.219    144
        104.81   1.171     43
        103.31   1.154     61
        102.06   1.140     64
         96.88   1.082     37
         91.81   1.026    510
         89.25   0.997    372
         88.31   0.987    495
         84.38   0.943    202
         81.94   0.915   1000
         79.19   0.885    263
         77.94   0.871    226
         75.88   0.848    158
         74.50   0.832    191
         72.63   0.811    102
    


  • 1H NMR 399.65 MHz
    C14 H32 N2 0.04 ml : 0.5 ml CDCl3
    N,N'-dibutyl-1,6-hexanediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.590 B *1 1.49 C *1 1.47 D 1.34 E 1.01 F 0.916

         Hz     ppm     Int.
    

       1053.10   2.636     34
       1042.36   2.609    446
       1035.16   2.591    621
       1027.83   2.572    484
        601.81   1.506    169
        601.20   1.505    167
        595.09   1.490    293
        591.92   1.482    197
        587.77   1.471    276
        586.55   1.468    294
        579.35   1.450    219
        577.27   1.445    131
        572.27   1.432    110
        553.96   1.387     81
        546.88   1.369    208
        538.94   1.349    327
        533.57   1.336    360
        531.37   1.330    353
        526.25   1.317    159
        524.29   1.312    183
        517.33   1.295     60
        373.17   0.934    575
        365.72   0.916   1000
        358.52   0.898    509
    

in CDCl3



liquid film