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网站主页CAS数据库列表 4801-58-5更多图谱N-羟基哌啶(4801-58-5)红外图谱(IR1)

N-羟基哌啶

产品名称 N-羟基哌啶

CAS号4801-58-5

分子式C5H11NO

分子量101.15

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  • Mass

    MS-NW-5425          
    N-hydroxypiperidine
    C5H11NO             (Mass of molecular ion:    101)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       5.9
          17.0       8.3
          18.0      36.4
          26.0       7.6
          27.0      29.1
          28.0      46.7
          29.0      23.6
          30.0      14.8
          37.0       1.5
          38.0       3.0
          39.0      22.8
          40.0       5.8
          41.0      53.4
          42.0      46.2
          43.0      11.6
          44.0      12.5
          45.0      23.0
          46.0       7.1
          50.0       3.6
          51.0       5.1
          52.0       6.0
          53.0       7.4
          54.0      23.8
          55.0     100.0
          56.0      33.8
          57.0      17.0
          58.0       1.4
          59.0       6.1
          60.0      12.6
          65.0       1.0
          67.0       4.2
          68.0       7.3
          69.0       2.0
          70.0       5.3
          72.0       2.5
          73.0       6.3
          78.0       1.0
          79.0       4.6
          80.0       4.8
          81.0       3.0
          82.0      20.4
          83.0      48.0
          84.0      55.5
          85.0      21.9
          86.0       1.8
          97.0       1.1
          98.0       1.6
          99.0       3.3
         100.0      63.8
         101.0      33.5
         102.0       2.4
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C5 H11 N O 0.04 ml : 0.5 ml CDCl3
    N-hydroxypiperidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.2 B 3.253 C 2.449 D 1.736 E 1.58 F 1.56 G 1.15 J(B,C)=9.8HZ. J(C,D)=2.6HZ.

         Hz     ppm     Int.
    

       3260.62   8.159     42
       1322.02   3.308     39
       1321.53   3.307     42
       1321.29   3.307     42
       1320.68   3.305     45
       1319.95   3.303     48
       1318.85   3.301     52
       1318.48   3.300     53
       1317.14   3.296     61
       1315.43   3.292     74
       1304.69   3.265    791
       1300.17   3.254    460
       1294.92   3.241    849
       1000.12   2.503     41
        999.15   2.501     46
        998.29   2.498     51
        997.68   2.497     54
        991.09   2.480    507
        988.65   2.474    481
        984.86   2.465    201
        984.25   2.463    200
        978.88   2.450    895
        971.56   2.432    187
        968.38   2.424    524
        965.70   2.417    485
        719.97   1.802     39
        718.99   1.800     42
        717.65   1.796     48
        716.43   1.793     50
        715.09   1.790     58
        714.60   1.789     60
        714.23   1.788     60
        713.87   1.787     61
        710.57   1.778    112
        702.27   1.758    533
        701.90   1.757    531
        699.83   1.752    526
        697.39   1.746    426
        691.65   1.731    564
        688.96   1.724    691
        686.89   1.719    701
        674.93   1.689     56
        673.58   1.686     46
        672.61   1.683     47
        671.39   1.680     43
        670.90   1.679     42
        669.43   1.676     40
        668.09   1.672     42
        667.48   1.671     43
        667.11   1.670     40
        663.57   1.661     40
        661.99   1.657     39
        660.89   1.654     40
        660.28   1.653     39
        659.79   1.651     40
        658.69   1.649     43
        658.33   1.648     46
        657.35   1.645     45
        656.98   1.644     45
        655.40   1.640     55
        654.42   1.638     56
        654.05   1.637     58
        653.69   1.636     58
        651.98   1.632     69
        650.88   1.629     74
        642.21   1.607    391
        639.04   1.599    525
        637.08   1.595    450
        635.74   1.591    471
        627.44   1.570    978
        626.10   1.567   1000
        615.97   1.542    455
        612.30   1.533    562
        609.86   1.526    338
        603.27   1.510    174
        599.73   1.501    231
        595.95   1.492    121
        481.57   1.205     44
        478.76   1.198    112
        474.73   1.188    133
        471.80   1.181     79
        471.31   1.180     77
        470.34   1.177     82
        469.97   1.176     82
        466.55   1.168    245
        462.40   1.158    318
        459.47   1.150    203
        456.42   1.143    103
        454.10   1.137    241
        450.20   1.127    314
        446.17   1.117    134
        442.26   1.107     89
        439.58   1.100     58
        437.99   1.096     50
        437.50   1.095     52
        437.01   1.094     50
        436.40   1.092     52
    


  • 1H NMR 89.56 MHz
    C5 H11 N O 0.045 g : 0.5 ml CDCl3
    N-hydroxypiperidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.08 B 3.25 C 2.44 D 1.96 to 0.78

         Hz     ppm     Int.
    

        733.00   8.185     78
        732.19   8.176     89
        731.19   8.165    104
        730.19   8.154    124
        729.88   8.150    136
        724.25   8.087    404
        723.94   8.084    405
        716.81   8.004     97
        297.06   3.317    458
        287.06   3.206    625
        231.06   2.580    234
        230.50   2.574    234
        229.63   2.564    243
        227.75   2.543    304
        225.06   2.513    147
        224.75   2.510    139
        220.75   2.465    449
        220.13   2.458    455
        219.81   2.455    459
        219.31   2.449    455
        217.50   2.429    613
        213.31   2.382    150
        212.81   2.377    152
        212.13   2.369    171
        210.25   2.348    254
        209.94   2.345    259
        209.56   2.340    261
        208.81   2.332    256
        207.06   2.312    318
        165.25   1.846    121
        163.50   1.826    146
        160.63   1.794    254
        157.81   1.763    474
        153.63   1.716    704
        150.56   1.682   1000
        148.31   1.656    875
        147.75   1.650    874
        145.44   1.624    816
        140.44   1.569    499
        138.00   1.541    461
        137.69   1.538    462
        136.63   1.526    446
        136.06   1.520    445
        135.69   1.516    442
        133.00   1.486    515
        132.69   1.482    512
        132.38   1.479    504
        125.06   1.397    162
        124.19   1.387    163
        123.88   1.384    161
        122.00   1.363    199
        121.56   1.358    201
        121.06   1.352    195
        120.56   1.347    198
        118.94   1.329    245
        116.63   1.303    204
        115.13   1.286    170
        114.63   1.280    162
        113.81   1.271    157
        113.44   1.267    158
        112.56   1.257    163
        111.25   1.243    136
        110.44   1.234    130
        108.63   1.213    166
        107.94   1.206    156
        107.38   1.199    146
        106.75   1.192    145
        106.31   1.188    145
        105.06   1.174    176
        103.44   1.155    129
        102.94   1.150    121
        101.56   1.134    143
        100.94   1.128    145
        100.44   1.122    136
         99.94   1.116    137
         98.94   1.105    131
         98.56   1.101    131
         97.94   1.094    132
         96.25   1.075     96
         95.94   1.072     95
         95.63   1.068    100
         94.81   1.059    105
         94.31   1.054    110
         94.00   1.050    109
         92.88   1.038     93
         92.13   1.029     83
         91.56   1.023     86
         90.00   1.005     80
         89.50   1.000     89
    

in CDCl3



liquid film