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MassMS-NW-5336 1-hexen-3-ol C6H12O (Mass of molecular ion: 100)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.1 26.0 1.6 27.0 15.2 28.0 3.0 29.0 17.3 31.0 6.8 39.0 7.2 40.0 1.2 41.0 11.0 42.0 1.4 43.0 9.8 44.0 2.9 45.0 1.5 53.0 3.5 54.0 1.7 55.0 6.4 56.0 2.2 57.0 100.0 58.0 5.5 67.0 4.2 71.0 9.2 72.0 12.4 73.0 1.2 82.0 3.4 83.0 1.6 85.0 2.0
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C6 H12 O 0.05 ml : 0.5 ml CDCl3 1-hexen-3-ol 
Assign. Shift(ppm)
A 5.847 B 5.201 C 5.077 D 4.081 E 2.68 F 1.50 G 1.38 J 0.926 J(A,B)=17.2HZ. J(A,C)=10.4HZ. J(A,D)=6.2HZ.
Hz ppm Int.2354.61 5.892 137 2348.39 5.877 139 2344.24 5.866 151 2337.89 5.850 188 2337.40 5.849 195 2331.18 5.834 160 2327.03 5.823 168 2320.68 5.807 165 2088.38 5.226 190 2087.04 5.223 257 2086.67 5.222 251 2085.45 5.219 209 2071.17 5.183 172 2069.82 5.180 232 2069.46 5.179 223 2068.24 5.176 185 2035.77 5.094 198 2034.55 5.091 235 2034.06 5.090 222 2032.96 5.087 200 2025.39 5.068 183 2024.17 5.065 225 2023.68 5.064 217 2022.58 5.061 192 1641.85 4.109 34 1640.63 4.106 58 1639.53 4.103 46 1634.40 4.090 127 1633.79 4.089 121 1630.86 4.081 37 1627.93 4.074 136 1622.80 4.061 43 1621.58 4.058 68 1620.48 4.055 45 1068.36 2.674 189 626.95 1.569 30 625.24 1.565 35 620.48 1.553 32 618.90 1.549 96 616.33 1.543 53 613.40 1.535 101 612.06 1.532 91 609.50 1.526 113 608.03 1.522 74 606.69 1.519 92 604.61 1.513 103 603.88 1.512 91 601.44 1.505 90 600.34 1.503 45 599.49 1.501 68 598.14 1.497 131 595.46 1.490 119 593.26 1.485 106 591.43 1.480 81 589.48 1.475 223 583.74 1.461 139 581.91 1.457 59 580.20 1.452 48 578.61 1.448 55 576.54 1.443 114 574.71 1.439 58 573.61 1.436 53 572.27 1.432 52 571.17 1.430 56 569.34 1.425 119 568.12 1.422 63 566.28 1.417 50 563.96 1.412 86 562.26 1.407 127 561.28 1.405 87 559.33 1.400 74 556.64 1.393 95 554.93 1.389 105 554.08 1.387 95 552.61 1.383 70 551.64 1.381 52 550.78 1.379 71 549.56 1.376 76 547.61 1.371 114 545.90 1.366 86 543.46 1.360 77 542.72 1.358 65 541.63 1.356 69 540.28 1.352 85 538.94 1.349 86 536.13 1.342 54 534.79 1.339 38 533.08 1.334 69 531.98 1.332 51 526.00 1.317 37 383.67 0.961 33 377.20 0.944 556 369.87 0.926 1000 365.60 0.915 107 362.67 0.908 421 358.40 0.897 43 357.42 0.895 34 356.20 0.892 39
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1H NMR 89.56 MHz C6 H12 O 0.04 ml : 0.5 ml CDCl3 1-hexen-3-ol Assign. Shift(ppm)
A 5.842 B 5.21 C 5.06 D 4.08 E 2.04 F 1.50 G 1.38 J 0.93
Hz ppm Int.543.00 6.063 117 536.88 5.995 126 532.88 5.950 150 526.88 5.883 168 525.75 5.871 205 519.69 5.803 215 515.63 5.758 253 509.63 5.691 283 475.19 5.306 237 474.00 5.293 263 473.25 5.285 355 472.13 5.272 331 461.25 5.151 295 460.13 5.138 309 459.31 5.129 237 458.19 5.117 266 456.75 5.100 208 456.00 5.092 184 454.88 5.080 188 451.19 5.038 200 450.00 5.025 224 449.25 5.017 199 448.13 5.004 190 375.81 4.197 41 369.69 4.128 128 363.56 4.060 134 357.38 3.991 54 183.00 2.044 1000 134.25 1.499 308 133.25 1.488 322 131.38 1.467 395 130.06 1.453 435 129.13 1.442 356 89.81 1.003 283 83.25 0.930 575 81.88 0.915 287 80.81 0.903 326
in CDCl3
liquid film
4880 A,200 M,liquid
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