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网站主页CAS数据库列表 4769-97-5更多图谱4-硝基吲哚(4769-97-5)核磁图(13CNMR)

4-硝基吲哚

产品名称 4-硝基吲哚

CAS号4769-97-5

分子式C8H6N2O2

分子量162.15

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  • Mass

    MS-NW-7527          
    4-nitroindole
    C8H6N2O2            (Mass of molecular ion:    162)
    

       Source Temperature: 200 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          28.0       3.1
          30.0       1.9
          37.0       1.6
          38.0       2.3
          39.0       5.7
          50.0       3.3
          51.0       3.9
          52.0       2.4
          61.0       2.5
          62.0       9.8
          63.0      15.6
          64.0       3.2
          65.0       2.5
          74.0       1.8
          75.0       2.4
          76.0       3.9
          77.0       4.6
          78.0       2.0
          85.0       1.0
          86.0       2.4
          87.0       3.8
          88.0       5.6
          89.0      39.9
          90.0       6.1
         103.0       1.9
         104.0      18.2
         105.0       1.7
         114.0       2.9
         115.0       6.3
         116.0      75.7
         117.0       7.4
         131.0       1.4
         132.0      15.8
         133.0       1.6
         146.0       1.2
         162.0     100.0
         163.0      10.3
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C8 H6 N2 O2 0.024 g : 0.5 ml DMSO-d6
    4-nitroindole
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.0 B 8.084 C 7.928 D 7.792 E 7.236 F 7.077

         Hz     ppm     Int.
    

       4796.21  12.002    204
       3236.55   8.099    661
       3235.82   8.097    887
       3231.79   8.087     77
       3231.42   8.086     77
       3228.49   8.079    701
       3227.76   8.077    921
       3173.73   7.942    430
       3172.99   7.940    785
       3172.08   7.938    720
       3165.85   7.922    451
       3164.93   7.920    882
       3164.02   7.917    737
       3114.38   7.793    733
       3112.37   7.788    535
       2935.43   7.346    552
       2930.48   7.333     71
       2927.37   7.325   1000
       2922.42   7.313     56
       2919.49   7.306    489
       2829.01   7.079    667
       2827.91   7.076    660
    

in DMSO-d6



KBr disc



nujol mull