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MassMS-KW-0526 alpha-allyl-alpha-methylbenzyl alcohol C11H14O (Mass of molecular ion: 162)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.2 18.0 3.1 27.0 1.9 39.0 6.3 41.0 4.3 43.0 100.0 44.0 2.3 50.0 2.2 51.0 7.6 52.0 1.5 63.0 2.0 65.0 2.4 66.0 1.4 71.0 1.3 76.0 1.1 77.0 13.6 78.0 3.4 91.0 3.4 102.0 1.6 103.0 7.4 105.0 8.6 115.0 3.7 121.0 71.4 122.0 6.3 127.0 3.3 128.0 11.5 129.0 21.1 130.0 2.4 141.0 1.4 143.0 5.8 144.0 12.2 145.0 2.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C11H14O 0.05 ml : 0.5 ml CDCl3 2-phenyl-4-penten-2-ol 
Assign. Shift(ppm)
A 7.408 B 7.298 C 7.200 D 5.602 E 5.07 F 5.06 G *1 2.631 J *1 2.471 K 2.36 L 1.509
Hz ppm Int.2966.80 7.422 209 2965.34 7.418 248 2963.38 7.413 94 2958.26 7.400 298 2957.16 7.397 280 2925.30 7.318 181 2923.34 7.313 81 2917.97 7.299 303 2916.51 7.296 171 2911.50 7.283 96 2909.92 7.279 179 2885.50 7.218 83 2884.16 7.215 131 2882.94 7.212 80 2878.79 7.201 69 2876.84 7.196 161 2874.88 7.192 56 2870.85 7.182 47 2869.63 7.178 68 2868.41 7.175 40 2261.60 5.658 35 2255.13 5.641 42 2253.42 5.637 44 2251.35 5.632 41 2246.95 5.621 44 2244.76 5.615 78 2243.29 5.612 50 2238.04 5.599 55 2236.58 5.595 78 2234.38 5.589 50 2229.86 5.578 48 2227.91 5.573 52 2226.20 5.569 51 2219.73 5.553 45 2030.52 5.080 138 2029.18 5.076 103 2021.37 5.057 171 2020.27 5.054 196 1062.99 2.659 60 1056.52 2.643 61 1049.20 2.625 88 1042.73 2.609 85 997.44 2.495 101 989.26 2.475 102 983.65 2.461 70 975.59 2.441 68 943.00 2.359 89 602.91 1.509 1000
in CDCl3
Liquid film
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