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MS-IW-7455 N-methyl-1-naphthylamine hydrochloride C11H11N HCl (Mass of molecular ion: 157)
Source Temperature: 120 °C Sample Temperature: 100 °C Direct, 75 eV
36.0 8.5 38.0 2.9 51.0 1.7 63.0 2.8 64.0 1.5 65.0 2.5 74.0 1.2 75.0 1.6 76.0 1.0 76.5 2.1 77.0 6.2 77.5 7.4 78.0 4.1 78.5 5.2 89.0 1.7 101.0 1.5 113.0 1.1 114.0 1.4 115.0 19.4 116.0 3.0 126.0 3.0 127.0 7.9 128.0 16.6 129.0 17.4 130.0 3.0 140.0 1.7 141.0 1.0 142.0 5.6 154.0 6.1 155.0 3.2 156.0 38.4 157.0 100.0 158.0 12.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H11 N 0.040 g : 0.5 ml CDCl3 N-methyl-1-naphthylamine hydrochloride Assign. Shift(ppm)
A 12.0 B 8.456 C 7.992 D 7.908 E 7.896 F 7.694 G 7.578 J 7.467 K 3.244
Hz ppm Int.
4789.07 11.984 30 3384.37 8.469 88 3383.63 8.467 93 3375.94 8.448 95 3375.03 8.445 99 3198.45 8.004 103 3197.54 8.001 121 3191.13 7.985 119 3190.03 7.983 127 3165.30 7.921 91 3160.35 7.908 105 3157.06 7.900 110 3156.69 7.899 104 3151.93 7.887 114 3083.79 7.717 50 3082.51 7.714 54 3076.83 7.699 72 3075.37 7.696 99 3074.08 7.692 57 3068.22 7.678 66 3067.12 7.675 65 3035.98 7.597 70 3035.07 7.595 76 3029.02 7.580 61 3027.93 7.577 105 3026.83 7.574 76 3020.78 7.559 51 3019.87 7.557 52 2992.02 7.487 116 2984.51 7.468 123 2983.78 7.466 128 2976.27 7.448 102 1296.82 3.245 1000
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