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4-氯丁酰氯

产品名称 4-氯丁酰氯

CAS号4635-59-0

分子式C4H6Cl2O

分子量141

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  • Mass

    MS-NW-2824          
    4-chlorobutyryl chloride
    C4H6Cl2O            (Mass of molecular ion:    140)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          14.0       1.8
          15.0       2.0
          26.0       5.8
          27.0      23.4
          28.0       5.7
          29.0       1.0
          35.0       2.4
          36.0       7.3
          37.0       3.2
          38.0       5.0
          39.0      30.3
          40.0       4.1
          41.0      86.3
          42.0      18.7
          43.0       1.7
          48.0       1.0
          49.0      16.1
          51.0       5.4
          55.0      21.2
          56.0       1.4
          61.0       1.9
          62.0       1.4
          63.0       8.1
          65.0       2.5
          69.0       7.7
          75.0       3.7
          76.0       5.1
          77.0      19.7
          78.0      48.4
          79.0       6.8
          80.0      15.4
         104.0       7.5
         105.0     100.0
         106.0       6.8
         107.0      32.0
         108.0       1.4
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C4 H6 Cl2 O 0.05 ml : 0.5 ml CDCl3
    4-chlorobutyryl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.605 B 3.12 C 2.17

         Hz     ppm     Int.
    

        329.38   3.678    514
        327.69   3.659     31
        326.81   3.650     37
        326.13   3.642     31
        323.31   3.610   1000
        319.19   3.564     52
        317.00   3.540    649
        287.31   3.209    344
        286.75   3.202    318
        280.25   3.130    724
        276.81   3.091     34
        273.25   3.052    506
        272.81   3.047    463
        206.94   2.311    124
        206.13   2.302    127
        200.31   2.237    325
        199.25   2.225    242
        197.69   2.208     40
        196.94   2.199     42
        194.06   2.167    323
        193.56   2.162    415
        192.75   2.153    317
        190.63   2.129     38
        189.88   2.121     33
        187.44   2.093    277
        186.69   2.085    190
        185.88   2.076    174
        180.56   2.017     81
        179.75   2.008     78
    

in CDCl3



liquid film