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MS-NW-3787 1,5-pentanediamine C5H14N2 (Mass of molecular ion: 102)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
17.0 1.1 18.0 7.2 27.0 2.3 28.0 5.6 29.0 1.8 30.0 100.0 31.0 2.7 39.0 1.5 41.0 3.9 42.0 3.1 43.0 6.6 44.0 2.5 45.0 7.3 55.0 3.3 56.0 26.0 57.0 2.3 59.0 1.6 68.0 1.1 72.0 2.3 73.0 4.8 83.0 1.0 84.0 2.0 85.0 6.7 86.0 1.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H14 N2 0.04 ml : 0.5 ml CDCl3 1,5-pentanediamine Assign. Shift(ppm)
A 2.683 B 1.53 to 1.37 C 1.26
Hz ppm Int.
247.19 2.761 83 246.75 2.756 87 244.69 2.733 86 242.06 2.703 129 240.69 2.688 296 237.13 2.648 62 234.13 2.615 154 137.25 1.533 74 136.19 1.521 60 135.00 1.508 41 132.75 1.483 103 131.25 1.466 89 129.44 1.446 177 127.50 1.424 258 126.56 1.414 272 125.94 1.407 222 125.31 1.400 234 124.81 1.394 240 122.81 1.372 282 118.94 1.329 31 118.31 1.322 34 112.44 1.256 1000
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