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MassMS-IW-8148 1-bromo-3,5-difluorobenzene C6H3BrF2 (Mass of molecular ion: 192)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
31.0 2.3 37.0 1.8 38.0 1.1 50.0 3.2 56.0 1.7 57.0 1.6 61.0 3.6 62.0 6.7 63.0 28.6 64.0 1.5 68.0 4.9 69.0 2.0 73.0 1.1 74.0 3.6 75.0 1.4 81.0 2.8 87.0 1.1 92.0 2.1 93.0 4.9 94.0 2.5 96.0 3.6 97.0 3.6 112.0 6.1 113.0 91.1 114.0 6.1 192.0 100.0 193.0 6.9 194.0 99.0 195.0 6.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H3 Br F2 0.05 ml : 0.5 ml CDCl3 1-bromo-3,5-difluorobenzene 
Assign. Shift(ppm)
A 7.047 B 6.756
Hz ppm Int.2827.88 7.076 96 2825.44 7.070 197 2823.00 7.064 210 2821.04 7.059 978 2819.95 7.057 508 2818.73 7.053 1000 2817.75 7.051 500 2815.55 7.046 462 2814.45 7.043 960 2813.23 7.040 508 2812.13 7.037 973 2810.18 7.032 222 2807.86 7.026 216 2805.30 7.020 111 2711.55 6.785 241 2709.23 6.780 427 2706.91 6.774 224 2705.32 6.770 37 2704.71 6.768 38 2702.64 6.763 460 2700.32 6.757 791 2698.00 6.751 429 2693.60 6.740 246 2691.41 6.735 428 2689.09 6.729 227
in CDCl3
liquid film
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