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MS-NW-6445 ethyl cyclopropanecarboxylate C6H10O2 (Mass of molecular ion: 114)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.0 26.0 2.0 27.0 9.3 28.0 1.1 29.0 24.0 31.0 1.3 38.0 1.7 39.0 17.1 40.0 3.5 41.0 33.9 42.0 7.4 43.0 2.9 45.0 6.2 55.0 3.7 57.0 1.0 58.0 5.7 59.0 1.0 68.0 5.0 69.0 100.0 70.0 5.2 71.0 2.7 73.0 2.8 83.0 1.2 85.0 6.6 86.0 23.2 87.0 12.3 99.0 1.6 114.0 3.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H10 O2 0.05 ml : 0.5 ml CDCl3 ethyl cyclopropanecarboxylate Assign. Shift(ppm)
A 4.130 B 1.596 C 1.263 D 0.958 E 0.845
Hz ppm Int.
1661.25 4.157 232 1654.17 4.140 592 1646.97 4.122 618 1639.89 4.104 244 650.39 1.628 58 645.75 1.616 117 642.46 1.608 121 641.11 1.605 81 637.70 1.596 230 634.28 1.588 83 633.18 1.585 132 629.64 1.576 131 625.00 1.564 70 511.96 1.282 634 509.40 1.275 38 504.76 1.264 1000 497.68 1.246 643 399.05 0.999 91 394.29 0.987 292 391.48 0.980 351 390.38 0.977 230 389.65 0.975 270 387.94 0.971 192 386.84 0.968 334 383.42 0.960 123 382.81 0.958 106 346.19 0.867 120 345.58 0.865 110 342.41 0.857 341 339.48 0.850 243 338.38 0.847 214 334.35 0.837 341 331.30 0.829 244 327.03 0.819 93
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