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网站主页CAS数据库列表 459-19-8更多图谱4-氟苯乙胺(459-19-8)核磁图(1HNMR)

4-氟苯乙胺

产品名称 4-氟苯乙胺

CAS号459-19-8

分子式C8H11ClFN

分子量175.63


  • Mass

    MS-NW-8745          
    4-fluorophenethylamine hydrochloride
    C8H10FN HCl         (Mass of molecular ion:    139)
    

       Source Temperature: 190 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          18.0       1.0
          28.0       1.8
          30.0     100.0
          31.0       1.5
          35.0       1.0
          36.0      11.2
          38.0       3.8
          39.0       1.0
          57.0       1.4
          63.0       1.0
          83.0       3.6
         101.0       1.1
         107.0       1.0
         109.0       9.2
         110.0       3.0
         123.0       2.7
         139.0       3.4
         152.0       3.2
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C8 H10 F N 0.039 g : 0.5 ml DMSO-d6
    4-fluorophenethylamine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.40 B 7.333 C 7.163 D 3.022 E 2.961

         Hz     ppm     Int.
    

       3356.69   8.400    286
       2938.35   7.353    421
       2936.16   7.347    201
       2932.74   7.339    498
       2929.69   7.331    590
       2926.27   7.323    256
       2924.07   7.317    525
       2921.14   7.310     74
       2874.39   7.193     88
       2871.34   7.185    622
       2869.14   7.180    203
       2864.75   7.169    239
       2862.43   7.163   1000
       2860.11   7.157    229
       2857.91   7.152     77
       2855.59   7.146    182
       2853.52   7.141    495
       2850.34   7.133     58
       1219.24   3.051    155
       1216.67   3.045    180
       1212.28   3.034    281
       1210.69   3.030    323
       1209.84   3.028    324
       1207.52   3.022    325
       1206.30   3.019    272
       1203.00   3.011    473
       1201.54   3.007    519
       1195.80   2.993     41
       1189.70   2.977    469
       1184.45   2.964    293
       1181.27   2.956    312
       1174.80   2.940    153
       1172.49   2.934    128
    

in DMSO-d6



KBr disc



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