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MS-NW-5672 4'-fluoropropiophenone C9H9FO (Mass of molecular ion: 152)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 2.6 28.0 1.1 29.0 2.7 50.0 2.5 51.0 1.8 57.0 1.8 68.0 1.1 69.0 2.0 74.0 1.6 75.0 9.9 76.0 1.0 94.0 2.0 95.0 35.3 96.0 2.7 123.0 100.0 124.0 7.8 152.0 8.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H9 F O 0.04 ml : 0.5 ml CDCl3 4'-fluoropropiophenone Assign. Shift(ppm)
A 7.982 B 7.115 C 2.967 D 1.222
Hz ppm Int.
722.63 8.069 207 720.44 8.045 71 717.19 8.008 211 715.75 7.992 85 715.00 7.984 74 713.56 7.968 258 710.38 7.932 74 708.13 7.907 251 705.31 7.876 31 648.38 7.240 30 645.63 7.209 290 643.38 7.184 78 640.00 7.147 34 638.75 7.133 67 637.19 7.115 375 636.56 7.108 283 635.00 7.091 82 633.69 7.076 31 630.31 7.038 68 628.13 7.014 221 277.25 3.096 101 269.75 3.012 372 262.44 2.931 405 255.56 2.854 134 116.31 1.299 449 109.19 1.220 1000 101.81 1.137 355
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