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网站主页CAS数据库列表 454-93-3更多图谱3-(fluorosulphonyl)benzoyl chloride (454-93-3)质谱(MS)

3-(fluorosulphonyl)benzoyl chloride

产品名称 3-(fluorosulphonyl)benzoyl chloride

CAS号454-93-3

分子式C7H4ClFO3S

分子量222.6212632


  • Mass

    MS-IW-0586          
    m-(fluorosulfonyl)benzoyl chloride
    C7H4ClFO3S          (Mass of molecular ion:    222)
    

       Source Temperature: 270 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          28.0       2.2
          36.0       1.2
          37.0       1.1
          38.0       2.9
          50.0      12.7
          51.0       1.3
          52.0       1.0
          63.0       2.6
          64.0       5.0
          73.0       1.2
          74.0       6.2
          75.0      18.4
          76.0      11.1
          80.0       1.4
          83.0       3.2
          92.0      29.2
          93.0       2.1
          95.0       5.2
         104.0       1.5
         111.0       1.4
         159.0      12.8
         187.0     100.0
         188.0       8.6
         189.0       5.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H4 Cl F O3 S 0.05 ml : 0.5 ml CDCl3
    m-(fluorosulfonyl)benzoyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.730 B 8.561 C 8.360 D 7.935

         Hz     ppm     Int.
    

       3495.64   8.747     22
       3490.75   8.735    581
       3488.92   8.730   1000
       3487.09   8.726    584
       3426.06   8.573    337
       3424.84   8.570    475
       3423.61   8.567    330
       3416.90   8.550    501
       3415.68   8.547    344
       3346.71   8.375    373
       3345.18   8.371    435
       3343.66   8.367    361
       3338.62   8.354    397
       3337.25   8.351    456
       3335.72   8.347    378
       3179.17   7.955    390
       3171.23   7.936    690
       3163.30   7.916    334
    

in CDCl3



liquid film