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3,4-二甲基氟苯

产品名称 3,4-二甲基氟苯

CAS号452-64-2

分子式C8H9F

分子量124.16

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  • Mass

    MS-IW-8154          
    4-fluoro-o-xylene
    C8H9F               (Mass of molecular ion:    124)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       1.2
          39.0       2.0
          50.0       1.9
          51.0       4.6
          57.0       2.8
          60.0       1.2
          61.0       1.6
          62.0       1.0
          63.0       2.0
          70.0       1.1
          74.0       1.1
          75.0       2.6
          77.0       7.1
          81.0       1.3
          83.0       6.0
          95.0       2.0
          96.0       3.8
          97.0       2.9
         101.0       4.3
         102.0       1.4
         103.0       7.6
         107.0       1.7
         109.0     100.0
         110.0       7.9
         120.0       1.0
         121.0       3.1
         122.0       2.8
         123.0      30.2
         124.0      56.1
         125.0       5.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H9 F 0.05 ml : 0.5 ml CDCl3
    4-fluoro-o-xylene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.002 B 6.794 C 6.740 D *1 2.188 E *1 2.163

         Hz     ppm     Int.
    

       2806.03   7.022    111
       2799.93   7.006    127
       2797.73   7.001    137
       2791.75   6.986    126
       2721.44   6.810    120
       2718.75   6.803    140
       2711.79   6.786    120
       2709.11   6.779    141
       2703.13   6.764     92
       2700.32   6.757     73
       2694.58   6.743    155
       2691.89   6.736    123
       2686.16   6.722     77
       2683.47   6.715     62
        874.39   2.188   1000
        864.62   2.164    851
    

in CDCl3



liquid film