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网站主页CAS数据库列表 446-33-3更多图谱5-氟-2-硝基甲苯(446-33-3)核磁图(13CNMR)

5-氟-2-硝基甲苯

产品名称 5-氟-2-硝基甲苯

CAS号446-33-3

分子式C7H6FNO2

分子量155.13

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  • Mass

    MS-NW-5445          
    5-fluoro-2-nitrotoluene
    C7H6FNO2            (Mass of molecular ion:    155)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          18.0       1.0
          27.0       1.4
          28.0       4.4
          29.0       1.6
          30.0       3.5
          31.0       3.1
          33.0       1.1
          37.0       1.7
          38.0       2.6
          39.0       9.8
          50.0       5.5
          51.0       8.1
          52.0       1.5
          56.0       1.5
          57.0      17.1
          58.0       1.1
          59.0       5.6
          61.0       2.4
          62.0       5.9
          63.0      14.2
          64.0       2.0
          68.0       1.6
          69.0       1.8
          70.0       2.6
          71.0       1.3
          74.0       2.3
          75.0       3.8
          76.0       1.0
          77.0       7.6
          81.0       6.9
          82.0       6.2
          83.0      71.9
          84.0       7.8
          85.0       1.4
          86.0       1.5
          87.0       1.3
          89.0       6.6
          90.0       6.9
          94.0       1.7
          95.0       7.4
          96.0       4.8
          97.0       4.1
         105.0       1.1
         107.0      17.2
         108.0       7.5
         109.0      34.6
         110.0      30.3
         111.0       6.4
         125.0       1.5
         138.0     100.0
         139.0       9.2
         155.0      12.5
         156.0       1.1
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H6 F N O2 0.05 ml : 0.5 ml CDCl3
    5-fluoro-2-nitrotoluene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.060 B 7.04 C 7.04 D 2.625

         Hz     ppm     Int.
    

       3229.25   8.081     37
       3228.03   8.078     77
       3226.56   8.074     61
       3222.90   8.065     86
       3220.21   8.058     82
       3218.63   8.054     84
       3217.41   8.051     39
       3215.94   8.047     36
       3213.13   8.040     86
       2819.70   7.056    220
       2819.09   7.054    232
       2818.48   7.053    148
       2817.63   7.051     87
       2814.58   7.043     31
       2813.96   7.042     35
       2811.40   7.035    265
       2809.33   7.030    114
       2808.59   7.028    120
       2804.32   7.017     78
       2803.83   7.016     79
       2801.51   7.010     41
       2801.03   7.009     39
       1049.19   2.626   1000
    


  • 1H NMR 89.56 MHz
    C7 H6 F N O2 0.04 ml : 0.5 ml CDCl3
    5-fluoro-2-nitrotoluene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.05 B 7.03 C 7.02 D 2.626

         Hz     ppm     Int.
    

        728.94   8.140     65
        723.75   8.082     76
        719.19   8.031    105
        713.88   7.971     93
        636.44   7.107    135
        635.81   7.100    167
        635.06   7.091    113
        634.31   7.083     63
        633.56   7.075     80
        632.88   7.067     79
        632.25   7.060     50
        631.75   7.054     46
        631.13   7.048     38
        628.88   7.022    124
        628.38   7.017    117
        627.69   7.009     77
        627.00   7.001    105
        626.31   6.994    109
        624.69   6.976     79
        624.00   6.968     82
        622.38   6.950     37
        621.81   6.943     70
        621.25   6.937     71
        235.19   2.627   1000
    

in CDCl3



liquid film



4880 A,200 M,liquid