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MS-IW-1265 2'-fluoroacetophenone C8H7FO (Mass of molecular ion: 138)
Source Temperature: 240 °C Sample Temperature: 160 °C Reservoir, 75 eV
39.0 1.0 43.0 10.3 50.0 2.8 51.0 1.9 57.0 1.3 61.5 1.3 62.0 1.0 63.0 1.1 68.0 1.5 69.0 2.4 74.0 2.1 75.0 10.5 76.0 1.0 83.0 1.0 94.0 1.9 95.0 33.4 96.0 4.8 109.0 1.0 123.0 100.0 124.0 7.8 138.0 24.3 139.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H7 F O 0.05 ml : 0.5 ml CDCl3 2'-fluoroacetophenone Assign. Shift(ppm)
A 7.858 B 7.503 C 7.203 D 7.115 E 2.621
Hz ppm Int.
3149.17 7.880 92 3147.71 7.877 89 3147.34 7.876 98 3141.72 7.862 175 3139.77 7.857 185 3133.91 7.842 102 3132.32 7.838 101 3131.96 7.837 107 3010.50 7.533 58 3008.54 7.528 63 3005.37 7.521 62 3003.54 7.516 84 3003.17 7.515 99 3002.20 7.513 88 3001.22 7.510 91 3000.24 7.508 84 2998.05 7.502 78 2997.07 7.500 88 2996.22 7.498 95 2995.24 7.495 102 2994.87 7.494 112 2992.92 7.489 82 2989.75 7.481 75 2987.92 7.477 78 2886.84 7.224 140 2885.74 7.221 160 2879.52 7.206 159 2879.03 7.204 197 2878.42 7.203 214 2877.93 7.202 212 2871.70 7.186 125 2870.61 7.183 141 2853.52 7.141 115 2852.78 7.139 117 2852.42 7.138 110 2845.21 7.120 107 2844.48 7.118 111 2844.12 7.117 104 2842.29 7.112 123 2841.55 7.111 126 2841.19 7.110 119 2833.98 7.092 106 2833.25 7.090 110 2832.89 7.089 104 1053.10 2.636 41 1050.17 2.628 951 1045.29 2.616 1000 1041.99 2.608 62
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