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网站主页CAS数据库列表 445-03-4更多图谱2-氨基-5-氯三氟甲苯(445-03-4)核磁图(1HNMR)

2-氨基-5-氯三氟甲苯

产品名称 2-氨基-5-氯三氟甲苯

CAS号445-03-4

分子式C7H5ClF3N

分子量195.57

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  • Mass

    MS-NW-6372          
    4-chloro-2-(trifluoromethyl)aniline
    C7H5ClF3N           (Mass of molecular ion:    195)
    

       Source Temperature: 250 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          18.0       1.3
          20.0       1.0
          28.0       3.2
          31.0       1.5
          36.0       1.7
          37.0       2.1
          38.0       2.5
          39.0       2.3
          41.0       2.3
          44.5       1.6
          45.5       1.2
          46.0       1.2
          50.0       2.3
          51.0       1.8
          52.0       4.6
          56.0       1.1
          57.0       1.3
          61.0       2.7
          62.0       4.3
          62.5       1.5
          63.0       9.4
          64.0       2.5
          65.0       2.3
          66.0       1.5
          69.0       2.3
          69.5       1.0
          70.0       5.2
          70.5       1.7
          73.0       2.6
          74.0       2.7
          75.0       4.2
          77.5       1.6
          81.0       1.7
          83.0       1.2
          87.0       1.5
          87.5       4.2
          88.0       5.2
          88.5       1.5
          89.0       2.4
          90.0       3.2
          91.0       1.2
          95.0       1.5
          97.0       1.1
          97.5       2.3
          98.0       1.0
          99.0       2.8
         100.0       1.4
         110.0       1.7
         111.0       1.1
         112.0       2.5
         113.0       8.6
         114.0       2.3
         120.0       3.0
         125.0       2.5
         131.0       1.2
         132.0       5.0
         133.0       1.4
         136.0       1.1
         138.0       1.5
         139.0       2.2
         140.0       5.2
         145.0       1.5
         147.0       1.3
         148.0      56.8
         149.0       4.3
         150.0      18.5
         151.0       1.3
         156.0       2.4
         158.0       1.2
         160.0       2.1
         167.0       1.3
         174.0       1.4
         175.0      73.5
         176.0      15.4
         177.0      24.3
         178.0       5.1
         194.0       2.9
         195.0     100.0
         196.0       9.3
         197.0      32.4
         198.0       2.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H5 Cl F3 N 0.05 ml : 0.5 ml CDCl3
    4-chloro-2-(trifluoromethyl)aniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.380 B 7.205 C 6.629 D 4.15

         Hz     ppm     Int.
    

       2957.15   7.400     21
       2956.42   7.398     23
       2950.93   7.384    959
       2948.49   7.378   1000
       2942.87   7.364     26
       2942.38   7.363     24
       2885.50   7.221    504
       2884.89   7.219    502
       2883.06   7.214    476
       2882.45   7.213    451
       2876.83   7.199    534
       2876.22   7.197    537
       2874.39   7.193    518
       2873.78   7.191    497
       2653.56   6.640    862
       2644.78   6.618    809
       1658.81   4.151    242
    

in CDCl3



liquid film



4880 A,200 M,liquid