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MS-IW-7444 diphenoxymethane C13H12O2 (Mass of molecular ion: 200)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
39.0 3.9 50.0 2.3 51.0 10.9 63.0 1.3 65.0 3.6 66.0 1.6 76.0 1.1 77.0 62.2 78.0 5.1 79.0 18.6 80.0 1.2 94.0 8.3 107.0 100.0 108.0 8.0 141.0 1.2 200.0 35.9 201.0 5.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H12 O2 0.05 ml : 0.5 ml CDCl3 diphenoxymethane Assign. Shift(ppm)
A 7.262 B 7.088 C 6.993
Hz ppm Int.
2913.33 7.290 51 2911.13 7.285 276 2910.28 7.283 136 2908.94 7.279 123 2906.13 7.272 74 2903.69 7.266 402 2902.34 7.263 454 2900.02 7.257 91 2897.09 7.250 158 2895.02 7.244 416 2892.58 7.238 73 2839.48 7.105 95 2838.75 7.104 116 2837.40 7.100 410 2836.18 7.097 545 2835.45 7.095 306 2834.11 7.092 169 2830.57 7.083 156 2829.59 7.081 253 2828.49 7.078 425 2827.51 7.075 406 2824.95 7.069 59 2802.61 7.013 120 2801.51 7.010 195 2800.42 7.008 109 2795.53 6.995 152 2795.04 6.994 163 2794.19 6.992 319 2793.33 6.990 163 2787.96 6.977 99 2786.87 6.974 161 2785.77 6.971 89 2265.14 5.668 1000
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