图谱信息 供应商 相关产品
网站主页CAS数据库列表 4409-11-4更多图谱4-(4-氯苄基)吡啶(4409-11-4)质谱(MS)

4-(4-氯苄基)吡啶

产品名称 4-(4-氯苄基)吡啶

CAS号4409-11-4

分子式C12H10ClN

分子量203.67

展开


  • Mass

    MS-NW-6266          
    4-(p-chlorobenzyl)pyridine
    C12H10ClN           (Mass of molecular ion:    203)
    

       Source Temperature: 250 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          18.0       2.6
          26.0       1.2
          27.0       1.4
          28.0       2.6
          38.0       1.5
          39.0       6.6
          50.0       5.2
          51.0      11.4
          52.0       1.8
          54.0       2.7
          57.5       1.2
          61.0       1.0
          62.0       2.7
          63.0       7.5
          64.0       2.2
          65.0       3.2
          69.0       1.5
          69.5       2.3
          70.0       3.0
          70.5       2.5
          73.0       2.0
          74.0       2.7
          75.0       5.7
          76.0       2.0
          77.0       1.4
          78.0       2.9
          83.5       9.0
          84.0       1.8
          86.0       1.2
          87.0       1.7
          88.0       1.0
          89.0       8.5
          90.0       3.0
          91.0       1.0
          99.0       3.4
         101.0       1.7
         106.0       1.0
         111.0       6.3
         113.0       3.0
         114.0       2.1
         115.0       5.5
         125.0      21.1
         126.0       2.6
         127.0       7.3
         128.0       1.2
         138.0       1.1
         139.0      22.2
         140.0       5.8
         141.0       9.0
         142.0       1.1
         149.0       1.9
         166.0       6.7
         167.0      46.6
         168.0     100.0
         169.0      13.7
         175.0       1.0
         201.0       1.2
         202.0       8.5
         203.0      76.7
         204.0      13.0
         205.0      25.7
         206.0       3.6
         217.0       7.3
         218.0       1.2
         219.0       2.5
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C12 H10 Cl N 0.046 g : 0.5 ml CDCl3
    4-(p-chlorobenzyl)pyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.500 B 7.267 C 7.09 D 7.07 E 3.926 400MHZ : HSP-41-747

         Hz     ppm     Int.
    

        764.38   8.535    439
        762.75   8.517    280
        759.94   8.486    290
        758.38   8.468    487
        656.88   7.335    373
        654.56   7.309    152
        650.50   7.264    232
        648.19   7.238   1000
        646.19   7.216    190
        640.56   7.153    146
        638.75   7.133    767
        636.25   7.105    606
        634.63   7.087    291
        631.81   7.055    337
        630.25   7.038    615
        627.88   7.011     62
        351.56   3.926    956
    


  • 1H NMR 399.65 MHz
    C12 H10 Cl N 0.05 ml : 0.5 ml CDCl3
    4-(p-chlorobenzyl)pyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.487 B 7.250 C 7.08 D 7.06 E 3.894 90MHZ : HSP-02-726

         Hz     ppm     Int.
    

       3393.19   8.491    261
       3392.82   8.490    261
       3391.36   8.486    259
       3390.26   8.484    260
       2902.10   7.262    563
       2893.68   7.241    688
       2832.28   7.087    634
       2823.73   7.066    669
       2816.53   7.048    467
       1556.40   3.895   1000
    

in CDCl3



KBr disc



liquid film



nujol mull