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1-碘十二烷

产品名称 1-碘十二烷

CAS号4292-19-7

分子式C12H25I

分子量296.23

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  • Mass

    MS-IW-4528          
    1-iodododecane
    C12H25I             (Mass of molecular ion:    296)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       8.0
          28.0       2.9
          29.0      16.2
          39.0       7.0
          40.0       1.4
          41.0      44.3
          42.0       9.9
          43.0      83.6
          44.0       3.9
          53.0       2.8
          54.0       2.4
          55.0      35.5
          56.0      11.0
          57.0     100.0
          58.0       7.5
          67.0       2.4
          68.0       1.2
          69.0      15.7
          70.0       5.9
          71.0      90.1
          72.0       5.5
          83.0       6.0
          84.0       2.2
          85.0      61.8
          86.0       4.0
          97.0       2.9
          98.0       1.0
          99.0      17.8
         100.0       1.4
         113.0      12.8
         114.0       1.1
         127.0       5.6
         128.0       3.1
         135.0       5.8
         137.0       5.7
         149.0       1.0
         151.0       1.0
         155.0       6.2
         169.0      18.1
         170.0       2.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H25 I 0.05 ml : 0.5 ml CDCl3
    1-iodododecane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.178 B 1.816 C 1.38 D 1.31 to 1.28 E 1.26 F 0.879

         Hz     ppm     Int.
    

       1277.34   3.197    253
       1270.26   3.179    487
       1263.18   3.161    268
        740.84   1.854     47
        733.89   1.837    134
        726.68   1.819    170
        719.24   1.800    156
        712.04   1.782     66
        559.81   1.401     64
        552.73   1.384     90
        545.53   1.366     77
        539.06   1.349     41
        533.94   1.337     36
        533.69   1.336     36
        519.53   1.300    176
        504.64   1.263   1000
        361.82   0.906     22
        358.52   0.898    170
        351.81   0.881    502
        344.73   0.863    212
    

in CDCl3



liquid film