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MS-NW-9641 3-ethoxymethacrylaldehyde C6H10O2 (Mass of molecular ion: 114)
Source Temperature: 270 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 2.5 27.0 14.9 28.0 4.3 29.0 39.1 30.0 2.5 31.0 5.0 38.0 1.2 39.0 12.7 40.0 17.4 41.0 5.7 42.0 1.2 43.0 2.5 45.0 2.7 55.0 4.4 56.0 2.5 57.0 37.4 58.0 12.5 68.0 18.7 69.0 3.2 70.0 1.6 71.0 6.1 83.0 1.0 85.0 100.0 86.0 15.1 87.0 2.3 96.0 2.2 97.0 3.2 113.0 2.4 114.0 43.9 115.0 9.7
parameter in CDCl3
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1H NMR 300 MHz C6 H10 O2 0.05 ml : 0.5 ml CDCl3 3-ethoxymethacrylaldehyde Parameter ppm Hz
D(A) 9.222 D(B) 7.042 D(C) 1.669 J(B,C) 1.15 D(D) 4.187 D(E) 1.396 J(D,E) 7.10
Hz ppm Int.
2766.58 9.222 605 2114.30 7.048 106 2113.14 7.044 262 2112.13 7.040 262 2110.97 7.037 106 1266.86 4.223 149 1259.69 4.199 441 1252.67 4.176 449 1245.57 4.152 151 501.28 1.671 1000 500.20 1.667 999 425.86 1.420 456 418.83 1.396 910 411.74 1.372 441
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