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MS-NW-9690 4-chloro-4'-hydroxybenzophenone C13H9ClO2 (Mass of molecular ion: 232)
Source Temperature: 160 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 2.6 39.0 3.7 50.0 1.3 51.0 1.0 63.0 1.5 65.0 8.3 70.0 1.2 74.0 1.0 75.0 5.4 76.0 1.3 84.0 1.7 93.0 10.9 102.0 4.2 103.0 1.4 111.0 10.6 113.0 3.6 121.0 100.0 122.0 7.8 139.0 16.6 140.0 1.7 141.0 5.5 175.0 1.0 197.0 8.7 198.0 1.3 232.0 36.7 233.0 5.8 234.0 12.4 235.0 1.8
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C13 H9 Cl O2 0.033 g : 0.5 ml DMSO-d6 4-chloro-4'-hydroxybenzophenone Assign. Shift(ppm)
A 10.51 B 7.70 C 7.68 D 7.607 E 6.924
Hz ppm Int.
4200.44 10.511 190 3084.11 7.718 55 3081.67 7.711 413 3079.68 7.706 152 3075.10 7.695 237 3073.27 7.690 1000 3071.59 7.686 237 3066.71 7.674 170 3064.73 7.669 548 3061.98 7.662 73 3045.81 7.622 98 3043.52 7.616 654 3041.53 7.611 183 3036.96 7.600 151 3034.97 7.595 406 3032.68 7.589 57 2774.35 6.942 62 2771.61 6.936 546 2769.62 6.931 160 2764.89 6.919 156 2762.91 6.914 512 2760.01 6.907 61
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