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MassMS-KW-0586 N-methyl-4-nitrophthalimide C9H6N2O4 (Mass of molecular ion: 206)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
28.0 3.3 30.0 1.9 37.0 1.3 38.0 1.0 50.0 1.6 51.0 1.4 51.5 1.4 53.0 1.1 62.0 1.7 63.0 3.0 65.0 1.0 73.0 1.7 74.0 12.1 75.0 42.4 76.0 5.7 77.0 3.5 89.0 1.1 103.0 56.2 104.0 8.5 105.0 1.0 116.0 9.6 117.0 1.1 119.0 2.0 120.0 2.3 131.0 5.0 132.0 15.1 133.0 1.5 149.0 8.8 150.0 2.8 159.0 6.4 160.0 5.2 161.0 2.5 162.0 4.8 178.0 1.6 205.0 6.5 206.0 100.0 207.0 10.8 208.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C9H6N2O4 0.038 g : 0.5 ml CDCl3 N-methyl-4-nitrophthalimide 
Assign. Shift(ppm)
A 8.658 B 8.622 C 8.076 D 3.263
Hz ppm Int.3462.65 8.662 126 3462.04 8.660 132 3460.58 8.657 165 3459.97 8.655 147 3451.54 8.634 131 3449.59 8.629 93 3443.49 8.614 131 3441.53 8.609 105 3232.55 8.086 144 3231.94 8.085 137 3224.49 8.066 136 3223.88 8.065 128 1304.33 3.263 1000
in CDCl3
KBr disk
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