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MS-IW-9309 1-chloro-3-methoxy-2-propanol C4H9ClO2 (Mass of molecular ion: 124)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 7.7 27.0 3.3 28.0 2.0 29.0 10.1 31.0 5.8 33.0 1.7 36.0 3.3 38.0 1.2 39.0 1.1 41.0 1.1 42.0 1.4 43.0 17.6 44.0 12.1 45.0 100.0 46.0 3.4 49.0 1.6 57.0 1.1 58.0 2.9 75.0 18.8 79.0 2.3 81.0 1.2 88.0 7.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H9 Cl O2 0.05 ml : 0.5 ml CDCl3 1-chloro-3-methoxy-2-propanol Assign. Shift(ppm)
A 3.979 B *1 3.629 C *1 3.585 D 3.505 E 3.404 F 3.20
Hz ppm Int.
1601.44 4.008 35 1596.07 3.994 100 1590.70 3.981 135 1585.45 3.968 107 1580.08 3.954 42 1461.18 3.657 92 1455.81 3.643 86 1450.07 3.629 232 1444.70 3.615 217 1438.84 3.601 229 1432.98 3.586 214 1427.61 3.573 92 1421.88 3.558 85 1404.05 3.514 455 1399.17 3.501 316 1398.56 3.500 296 1360.72 3.405 1000 1277.59 3.197 214
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