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网站主页CAS数据库列表 4146-04-7更多图谱DL-2-氨基-1-戊醇(4146-04-7)质谱(MS)

DL-2-氨基-1-戊醇

产品名称 DL-2-氨基-1-戊醇

CAS号4146-04-7

分子式C5H13NO

分子量103.16


  • Mass

    MS-NW-7302          
    DL-2-amino-1-pentanol
    C5H13NO             (Mass of molecular ion:    103)
    

       Source Temperature: 200 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       2.0
          18.0       4.4
          27.0       5.1
          28.0       7.3
          29.0       5.7
          30.0      56.2
          31.0       3.7
          39.0       3.6
          41.0       5.0
          42.0      14.5
          43.0       5.6
          44.0       9.0
          55.0       7.4
          56.0       3.5
          57.0       2.4
          60.0      28.7
          70.0       1.1
          72.0     100.0
          73.0       5.1
          86.0       5.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C5 H13 N O 0.05 ml : 0.5 ml CDCl3
    DL-2-amino-1-pentanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 3.548 B *1 3.261 C 2.94 D 2.78 E 1.38 F 1.26 G 0.93 J(A,B)=-10.7HZ J(A,D)=3.9HZ J(B,D)=7.6HZ

         Hz     ppm     Int.
    

        326.81   3.650    102
        323.00   3.607    123
        316.25   3.532    220
        312.38   3.488    234
        300.69   3.358    229
        297.00   3.317     30
        296.50   3.311     31
        293.06   3.273    287
        290.06   3.239    112
        287.44   3.210     34
        286.94   3.204     35
        286.44   3.199     35
        285.88   3.193     34
        282.50   3.155    179
        263.00   2.937   1000
        120.75   1.349    395
         88.50   0.989    273
         82.88   0.926    572
         77.50   0.866    229
    

in CDCl3



liquid film