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MassMS-IW-2621 3,3-diethoxypropylamine C7H17NO2 (Mass of molecular ion: 147)
Source Temperature: 220 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 1.7 18.0 5.7 19.0 1.8 26.0 1.3 27.0 11.3 28.0 8.5 29.0 22.5 30.0 100.0 31.0 8.6 41.0 1.4 42.0 4.6 43.0 13.7 44.0 39.1 45.0 23.2 46.0 4.6 47.0 66.0 54.0 1.2 55.0 2.0 56.0 20.2 57.0 41.6 58.0 11.1 60.0 4.4 61.0 4.4 70.0 1.1 72.0 57.2 73.0 48.7 74.0 4.7 75.0 32.3 76.0 2.0 86.0 2.2 89.0 1.3 100.0 5.0 101.0 34.5 102.0 12.8 103.0 23.4 104.0 1.3 117.0 1.0 118.0 10.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H17 N O2 0.05 ml : 0.5 ml CDCl3 3,3-diethoxypropylamine 
Assign. Shift(ppm)
A 4.597 B *1 3.659 C *1 3.506 D 2.788 E 1.82 F 1.775 G 1.205
Hz ppm Int.1843.14 4.612 79 1837.40 4.598 160 1831.79 4.584 82 1478.76 3.701 44 1471.68 3.683 133 1469.36 3.677 66 1464.60 3.665 151 1462.28 3.659 182 1457.40 3.647 93 1455.20 3.642 184 1448.12 3.624 63 1416.26 3.544 56 1409.18 3.527 171 1406.86 3.521 53 1402.10 3.509 181 1399.78 3.503 142 1395.02 3.491 70 1392.70 3.485 140 1385.62 3.468 47 1121.22 2.806 155 1114.38 2.789 322 1107.67 2.772 173 727.42 1.821 33 724.98 1.815 34 718.87 1.799 114 713.26 1.785 126 712.16 1.782 209 706.42 1.768 200 705.32 1.765 128 699.71 1.751 96 489.01 1.224 550 481.81 1.206 1000 474.85 1.189 621
in CDCl3
liquid film
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